Solid-state preparation of hybrid organometallic-organic macrocyclic adducts with long chain dicarboxylic acids

被引：27
|
作者：
Braga, Dario [1 ]
Giaffreda, Stefano Luca [1 ]
Grepioni, Fabrizia [1 ]
机构：
[1] Univ Bologna, Dipartimento Chim G Ciamician, I-40126 Bologna, Italy
来源：
CHEMICAL COMMUNICATIONS | 2006年 / 37期
关键词：
D O I：
10.1039/b608691h
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The supramolecular macrocyclic adducts of general formula {[Fe(eta(5)-C5H4-C5H4N)(2)]center dot[HOOC(CH2)(n)COOH]}(2) with n = 4 (adipic acid), n = 6 (suberic acid), n = 7 (azelaic acid) and n = 8 (sebacic acid) have been obtained quantitatively by kneading powdered samples of the crystalline organometallic and organic reactants with drops of MeOH(for n = 4, 6 and 7) and by direct crystallization from MeOH for n = 8, while the adduct with n = 5 represents an isomeric open chain alternative to the macrocycle.
引用
收藏
页码：3877 / 3879
页数：3
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