Comparison of the Kjeldahl method and a combustion method for total nitrogen determination in animal feed

被引：113
|
作者：
Marcó, A
Rubio, R
Compañó, R
Casals, I
机构：
[1] Univ Barcelona, Dept Quim Analit, E-08028 Barcelona, Spain
[2] Univ Barcelona, Serv Cientificotecn, E-08028 Barcelona, Spain
来源：
TALANTA | 2002年 / 57卷 / 05期
关键词：
total nitrogen; Kjeldahl method; combustion method; animal feed;
D O I：
10.1016/S0039-9140(02)00136-4
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
The features of the Dumas combustion method (CM) and those of the Kjeldahl method (KM) were compared as they apply to total nitrogen determination in animal feed. Both methods achieved similar repeatability (S.D., 0.11-0.38 from Kjeldahl and 0.15-0.36 from combustion) and similar intra-laboratory reproducibility (S.D., 0.11-0.39 from Kjeldahl and 0.15-0.37 from combustion). R.S.D. is always below NO. These results show that the CM is suitable for the analysis of protein content in animal feed (5-75% protein content). The CM is recommended owing to its shorter analysis time, its cost and its environmental suitability. (C) 2002 Elsevier Science B.V. All rights reserved.
引用
收藏
页码：1019 / 1026
页数：8
相关论文
共 50 条
  • [1] Simplified Method for the Determination of Total Kjeldahl Nitrogen in Wastewater
    Hicks, Tristan D.
    Kuns, Caleb M.
    Raman, Chandrashekar
    Bates, Zane T.
    Nagarajan, Subhalakshmi
    ENVIRONMENTS, 2022, 9 (05)
  • [2] KJELDAHL METHOD FOR TOTAL NITROGEN
    KIRK, PL
    ANALYTICAL CHEMISTRY, 1950, 22 (02) : 354 - 358
  • [3] Protein nitrogen combustion method collaborative study I. Comparison with smalley total Kjeldahl nitrogen and combustion results
    Berner, David L., 1600, American Oil Chemists' Soc, Champaign, IL, United States (71):
  • [4] PROTEIN NITROGEN COMBUSTION METHOD COLLABORATIVE STUDY .1. COMPARISON WITH SMALLEY TOTAL KJELDAHL NITROGEN AND COMBUSTION RESULTS
    BERNER, DL
    BROWN, J
    JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1994, 71 (11) : 1291 - 1293
  • [5] PERCENTAGE OF NITRATE NITROGEN IN TOTAL NITROGEN-DETERMINATION BY KJELDAHL METHOD
    SCHARF, H
    ARCHIV FUR ACKER UND PFLANZENBAU UND BODENKUNDE-ARCHIVES OF AGRONOMY AND SOIL SCIENCE, 1989, 33 (03): : 159 - 168
  • [6] Improvement of the Conditions for the Determination of Total Nitrogen in Fish Meal in Kjeldahl Method and Its Comparison with Dumas Method
    Kubota, Takashi
    Oshida, Tomoko
    Yanai, Kozue
    Inoue, Yuzuru
    Matsui, Seiji
    Matsumoto, Takaharu
    Ishikuro, Eiichi
    Yasui, Akemi
    BUNSEKI KAGAKU, 2011, 60 (01) : 67 - 74
  • [7] The determination of nitrogen by the Kjeldahl method
    Gibson, RB
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1904, 26 (01) : 105 - 110
  • [8] TELLURIUM AS CATALYST IN SEMIMICRO KJELDAHL METHOD FOR TOTAL NITROGEN DETERMINATION
    LIAO, CFH
    JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 1982, 65 (04): : 786 - 790
  • [9] Method Performance Study of the Determination of Total Nitrogen in Soy Sauce by the Kjeldahl Method
    Shintaro Nozawa
    Akiko Hakoda
    Kenichi Sakaida
    Tadanao Suzuki
    Akemi Yasui
    Analytical Sciences, 2005, 21 : 1129 - 1132
  • [10] Optimum Conditions for the Determination of Total Nitrogen in Vinegar by the Kjeldahl Method
    Hashimoto, Yoshiko
    Chuda, Yoshihiro
    Suzuki, Tadanao
    Yasui, Akemi
    BUNSEKI KAGAKU, 2009, 58 (05) : 379 - 385
12345