Crystalline perfection, thermal, mechanical and optical investigations on solution grown-arginine monohydrochloride single crystal

被引:16
|
作者
Krishna, Anuj [1 ,2 ]
Sonia [1 ,2 ]
Vijayan, N. [2 ]
Verma, Sunil [3 ]
Singh, Budhendra [4 ,5 ]
Bidkin, Igor [4 ,5 ]
Jayalakshmy, M. S. [6 ]
Sridhar, B. [7 ]
Das, Subhasis [8 ]
机构
[1] Acad Sci & Innovat Res, CSIR Natl Phys Lab Campus,Dr KS Krishnan Rd, New Delhi 110012, India
[2] CSIR Natl Phys Lab, Xray Anal & Crystal Growth Sect, Dr KS Krishnan Rd, New Delhi 110012, India
[3] Raja Ramanna Ctr Adv Technol, Laser Mat Dev & Devices Div, Indore 452013, India
[4] Univ Aveiro, Dept Mech Engn, TEMA NRD, P-3810193 Aveiro, Portugal
[5] Univ Aveiro, AIN, P-3810193 Aveiro, Portugal
[6] Cochin Univ Sci & Technol, Cochin 682022, Kerala, India
[7] CSIR Indian Inst Chem Technol, Uppal Rd, Hyderabad 500007, Telangana, India
[8] Univ Burdwan, Dept Phys, Bardhaman 713104, India
关键词
DAMAGE THRESHOLD; MONOHYDRATE; HYDROCHLORIDE; DIFFRACTION; ACID;
D O I
10.1007/s10854-016-6054-4
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
In the present work we report crystallization and detailed analyses on l-arginine monohydrochloride single crystal an efficient material for nonlinear optical applications. The crystal of titled material was grown using slow evaporation solution growth technique using double distilled water as solvent. Single crystal X-ray diffraction technique revealed that lattice dimensions of grown crystal are in good agreement with the reported literature and it crystallised in monoclinic crystal system. High resolution X-ray diffraction study revealed that crystalline perfection is fairly good. Optical homogeneity and variation of birefringence across the sample cross-section was studied using birefringence interferometer. Specific heat and thermal conductivity of grown crystal was measured using photopyroelectric technique and was found to be higher than many organic and inorganic crystals. Its various mechanical properties and resistance toward deformation was examined using nano-indentation technique. Further laser damage threshold value and phase matching angle was also measured.
引用
收藏
页码:4306 / 4312
页数:7
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