Sonochemical Synthesis of Differently-Sized Nanoparticles of a Silver(I) Compound: An Optical, Anticancer, and Thermal Activity Evaluation Study

被引:4
|
作者
Ramezani, Bahman [1 ]
Hossein Shahverdizadeh, Gholam [1 ]
Edjlali, Ladan [1 ]
Ramezani, Fatemeh [2 ]
Babazadeh, Mirzaagha [1 ]
机构
[1] Islamic Azad Univ, Tabriz Branch, Dept Chem, Tabriz, Iran
[2] Sch Adv Med Sci, Dept Mol Med, Tabriz, Iran
来源
CHEMISTRYSELECT | 2020年 / 5卷 / 42期
关键词
Antitumor agent; MTT assay; Nanoparticles; Phase-pure silver nanoparticles; Sonochemical synthesis; ULTRASONIC-ASSISTED SYNTHESIS; ORGANIC FRAMEWORK; CARBON NANOTUBES; COMPLEXES; SPECTROSCOPY; DERIVATIVES; PRECURSORS; GREEN; SHAPE; GAP;
D O I
10.1002/slct.202003173
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Nano silver-based inorganic structure with the chemical formulation of [Ag(dafo)(2)(NO3)] (1), dafo=4,5-diazafluoren-9-one, was synthesized using sonochemical method. Three different ultrasonic generator output powers of 30 W, 60 W, 90 W, each in two different reaction temperature ranges of 0-10 degrees C and 25-35 degrees C, were our sonochemical reaction conditions. After preparing compound 1 with differently-sized nanoparticles under the sonochemical reaction conditions, we conducted an evaluation study into the optical, anti-cancer, and thermal activities of the compound. High ultrasonic generator output power and low reaction temperature were the two prevailing conditions that affected the size and purity of the nanoparticles of compound 1. Based on our identifying methods, nanoparticles of 90 W at 0-10 degrees C showed the lowest particles size among other nanoparticles. The best optical, anticancer, and thermal activities appertained to the nanoparticles. The nanoparticles were heated to 500 degrees C in an electric furnace to synthesize phase-pure silver nanoparticles.
引用
收藏
页码:13081 / 13090
页数:10
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