Microwave Assisted Synthesis and Characterization of Glycidyl Azide Polymers Containing Different Initiating Diol Units

被引：0
|
作者：
Kshirsagar, Ajay [1 ]
Gite, Vikas [1 ]
Hundiwale, Dilip [1 ]
Mahulikar, Pramod [1 ]
机构：
[1] North Maharashtra Univ, Sch Chem Sci, PB 80, Jalgaon 425001, MS, India
来源：
CENTRAL EUROPEAN JOURNAL OF ENERGETIC MATERIALS | 2015年 / 12卷 / 04期
关键词：
glycidyl azide polymer; poly(epichlorohydrin); cationic ring-opening polymerization; microwave irradiation; thermal properties; BISMUTH NITRATE PENTAHYDRATE; POLY(GLYCIDYL AZIDE); COPOLYMERS; SCIENCE; AGENT;
D O I：
暂无
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
Glycidyl azide polymers (GAPs), containing different initiating diol units were prepared by treating the corresponding poly(epichlorohydrins) (PECHs) with sodium azide under microwave irradiation (600 W power) at 80 degrees C, during 12 min. The PECHs containing different diol units were synthesized by the polymerization of epichlorohydrin using borontrifluoride etherate as initiator in the presence of small amounts of low molecular weight diols. The synthesized PECHs and GAPs, containing different initiating diol units, were characterized by various spectroscopic techniques and by thermal analysis (DSC). These results are reported and discussed.
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页码：757 / 767
页数：11
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