Isolation and Structural Elucidation of Secondary Metabolites from Dodonaea viscosa and Qualitative Screening of its Sub Fractions Based on GC-MS

被引:0
|
作者
Fatima, Mashhad [1 ]
Shah, Syed Shaukat Ali Muttaqi [2 ]
Anis, Itrat [1 ]
Zafar, Urooj [3 ]
Sadaf, Sohira [3 ]
Javed, Bisma [3 ]
机构
[1] Univ Karachi, Dept Chem, Karachi, Pakistan
[2] Univ Karachi, Dept Pharmaceut, Karachi, Pakistan
[3] Univ Karachi, Dept Microbiol, Karachi, Pakistan
来源
关键词
Dodonaea viscosa; GC-MS analysis; Antimicrobial activity; Phytochemical investigation; Minimum Bactericidal concentration; ESSENTIAL OIL; FLAVONOIDS; LINN; ACID;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A phytochemical investigation of Dodonaea viscosa plant extract was conducted. A new 3,5,7-trihydroxy-6,4'-dimethoxy-3'-isoprenyl-flavone (1) and three known compounds Hautriwaic lactone (2), Kamempferol 3-methyl ether (3) and vanillic acid (4) were isolated from the aerial parts of Dodonaea viscosa. The structure of the isolated constituents was elucidated using 1D and 2D Nuclear Magnetic Resonance (NMR) and mass spectrometry. The qualitative study of the Fraction 1 was performed by using Gas Chromatography (GC) and Gas Chromatography - Mass Spectrometry (GC-MS). The nature of compounds was confirmed by NIST library search. The antimicrobial activity and possible use of the plant extracts were also elaborated.
引用
收藏
页码:575 / 580
页数:6
相关论文
共 47 条
  • [1] ISOLATION AND IDENTIFICATION OF CHLORPROPHAM AND 2 OF ITS METABOLITES IN POTATOES BY GC-MS
    WOROBEY, BL
    SUN, WF
    CHEMOSPHERE, 1987, 16 (07) : 1457 - 1462
  • [2] A fast GC-MS screening procedure for ketamine and its metabolites in urine samples
    Lin, HR
    Lua, AC
    JOURNAL OF FOOD AND DRUG ANALYSIS, 2005, 13 (02) : 107 - 111
  • [3] GC/MS chemical profiling and isolation of secondary metabolites from Leontice ewersmannii
    Omirzakova, Nazgul
    Samy, Mamdouh Nabil
    Kiyekbayeva, Lashyn
    Datkhayev, Ubaidilla
    Akhtayeva, Nursulu
    Ross, Samir Anis
    NATURAL PRODUCT RESEARCH, 2024,
  • [4] Methods for isolation, purification and structural elucidation of bioactive secondary metabolites from marine invertebrates
    Ebada, Sherif S.
    Edrada, Ru Angelie
    Lin, Wenhan
    Proksch, Peter
    NATURE PROTOCOLS, 2008, 3 (12) : 1820 - 1831
  • [5] Methods for isolation, purification and structural elucidation of bioactive secondary metabolites from marine invertebrates
    Sherif S Ebada
    Ru Angelie Edrada
    Wenhan Lin
    Peter Proksch
    Nature Protocols, 2008, 3 : 1820 - 1831
  • [6] Screening of clostebol and its metabolites in bovine urine with ELISA and comparison with GC-MS results in an interlaboratory study
    Crabbe, P
    Meyer, UJ
    Zhi, ZL
    Pieraccini, G
    O'Keeffe, M
    Van Peteghem, C
    JOURNAL OF ANALYTICAL TOXICOLOGY, 2003, 27 (04) : 213 - 220
  • [7] Isolation, Structure Elucidation and Antioxidant Screening of Secondary Metabolites from Rhynchosia pseudo-cajan
    Riaz, Tauheeda
    Abbasi, Muhammad Athar
    Riaz, Naheed
    Aziz-Ur-Rehman
    Saleem, Muhammad
    Khan, Khalid Mohammed
    Ajaib, Muhammad
    JOURNAL OF THE CHEMICAL SOCIETY OF PAKISTAN, 2012, 34 (05): : 1204 - 1212
  • [8] Green extraction techniques with highly efficient non-conventional reactors: a screening of secondary metabolites by LC-MS and GC-MS
    Alexandru, L.
    Binello, A.
    Mantegna, S.
    Chemat, F.
    Cravotto, G.
    PLANTA MEDICA, 2013, 79 (13) : 1248 - 1248
  • [9] Isolation and Identification of Volatile Metabolites from the Biocontrol Agent Trichoderma harzianum through GC-MS Analysis
    Pandey, Sonika
    Srivastava, Mukesh
    Shahid, Mohammad
    Singh, Anuradha
    Trivedi, Shubha
    Kumar, Vipul
    Maurya, Manoj Kumar
    Srivastava, Yatindra Kumar
    JOURNAL OF PURE AND APPLIED MICROBIOLOGY, 2015, 9 : 553 - 559
  • [10] Isolation and Structural Elucidation of Nitrogenous Secondary Metabolites from Terrestrial and Marine Streptomyces spp.
    Shaaban, Mohamed
    Shaaban, Khaled A.
    Helmke, Elisabeth
    Gruen-Wollny, Iris
    Laatsch, Hartmut
    NATURAL PRODUCT COMMUNICATIONS, 2017, 12 (03) : 351 - 354