4-(Allylamino)-2-amino-6-benzyloxy-5-nitrosopyrimidine from synchrotron data at 150 K:: double chains built from N-H•••N,N-H•••O, N-H•••π(arene) and aromatic π-π-stacking interactions

被引：1

作者：

MacLean, EJ

Low, JN

Quesada, A

Melguizo, M

Nogueras, M

Glidewell, C ^{[1
]}

机构：

[1] Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland

[2] SERC, Daresbury Lab, CLRC, Warrington WA4 4AD, Cheshire, England

[3] Univ Aberdeen, Dept Chem, Old Aberdeen AB24 3UE, Scotland

[4] Univ Jaen, Dept Quim Inorgan & Organ, Jaen 23071, Spain

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY | 2002年 / 58卷

关键词：

D O I：

10.1107/S0108270102010387

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

In the title compound, C14H15N5O2, the intramolecular dimensions are consistent with a highly polarized electronic structure. The molecules are linked into chains by a combination of N-H...N, N-H...O and N-H...pi(arene) hydrogen bonds, and the chains are linked in pairs by aromatic pi-pi-stacking interactions.

引用

页码：o442 / O444

页数：3

共 50 条

[1] 2-amino-4,6-bis(benzyloxy)-5-nitroso-pyrimidine:: chains built from three-centre N-H •••(N,O) and N-H •••π(arene) hydrogen bonds
Quesada, A
Low, JN
Melguizo, M
Nogueras, M
Glidewell, C
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2002, 58 (06): : O355 - O358
[2] 2,4-dinitrophenylhydrazine, redetermined at 120 K:: a three-dimensional framework built from N-H ••• O, N-H ••• (O)2, N-H ••• π(arene) and C-H ••• O hydrogen bonds
Wardell, James L.
Low, John N.
Glidewell, Christopher
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2006, 62 : O318 - O320
[3] N-H•••N, N-H•••O and N-H•••πCO hydrogen bonding in [N,N-bis(2-amino-ethyl)-2-aminoethyl]ammonium tetra-carbonylcobaltate(1-)
Rivas, JCM
Brammer, L
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1998, 54 : 1799 - 1802
[4] Stacking and N-H • • • O interactions in 2,3-dimethyl-6-nitroaniline
Kruszynski, R
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O2379 - O2381
[5] Energetic aminated-azole assemblies from intramolecular and intermolecular N-H•••O and N-H•••N hydrogen bonds
He, Chunlin
Yin, Ping
Mitchell, Lauren A.
Parrish, Damon A.
Shreeve, Jean'ne M.
CHEMICAL COMMUNICATIONS, 2016, 52 (52) : 8123 - 8126
[6] Cocrystals of 6-propyl-2-thiouracil: N-H•••O versus N-H•••S hydrogen bonds
Tutughamiarso, Maya
Egert, Ernst
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2011, 67 : O439 - O445
[7] Bis(5-amino-3-methyl-1-phenyl-1H-pyrazol-4-yl)-3,4,5-trimethoxyphenylmethane:: sheets built from N-H ••• N and N-H ••• O hydrogen bonds
Low, JN
Cobo, J
Portilla, J
Quiroga, J
Glidewell, C
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2004, 60 : O1034 - O1037
[8] (Pyrazinecarbonyl)hydrazones of heteroarenealdehydes: crystal structures formed from N-H ... O, N-H ... N, C-H ... O hydrogen-bonds, C-H ... π and π ... π interactions
Howie, R. Alan
da Silva Lima, Camilo H.
Kaiser, Carlos R.
da Silva, Marcele M.
de Souza, Marcus V. N.
Wardell, James L.
Wardell, Solange M. S. V.
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-CRYSTALLINE MATERIALS, 2010, 225 (06): : 245 - 252
[9] Co-crystals of 5,6-Dimethyl-2-thiouracil: further proof of the robustness of the ADA-DAD N-H ••• O/N-H ••• N/N-H ••• S-synthon
Huetzler, Wilhelm Maximilian
Egert, Ernst
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2016, 72 : S377 - S377
[10] 5-Amino-1-benzoyl-3-methylpyrazole: complex sheets built from N-H•••N, C-H•••O and C-H•••π(arene) hydrogen bonds
Quiroga, Jairo
Portilla, Jaime
Hursthouse, Michael B.
Cobo, Justo
Glidewell, Christopher
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2010, 66 : O159 - O162

← 1 2 3 4 5 →