Synthesis and antioxidant properties of bis(3-(3,5-di-tert-butyl-4-hydroxyphenyl)propyl)phosphite

被引：0
|
作者：
Akhmadullin, R. M. [1 ]
Galiev, M. F. [2 ]
Nugumanova, G. N. [2 ]
Cherezova, E. N. [2 ]
Gazizov, A. S. [3 ]
Verizhnikov, L. V. [1 ]
Akhmadullina, A. G. [1 ]
Diachkov, I. M. [2 ]
机构：
[1] R&D AhmadullinS Sci & Technol, Kazan 420015, Russia
[2] Kazan Natl Res Technol Univ, Kazan, Russia
[3] AE Arbuzov Inst Organ & Phys Chem, Kazan, Russia
来源：
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2021年 / 196卷 / 07期
关键词：
Bis(3-(3; 5-di-tert-butyl-4-hydroxyphenyl)propyl)phosphite; synthesis; antioxidant properties; IR; NMR spectroscopy; 2; 2-diphenyl-1-picrylhydrazyl; thermal oxidation;
D O I：
10.1080/10426507.2021.1885034
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Bis(3-(3,5-di-tert-butyl-4-hydroxyphenyl)propyl)phosphite was synthesized by reaction of 2,6-di-tert-butyl-4-(3-hydroxyproyl)phenol with dibutyl phosphite. The structure of bis(3-(3,5-di-tert-butyl-4-hydroxyphenyl)propyl)phosphite was supported by IR and NMR (H-1, C-13, P-31) spectroscopy; its composition was confirmed by elemental analysis. High antioxidant activity of the synthesized phosphite has been shown in a model reaction with the free chromogen-radical 2,2-diphenyl-1-picrylhydrazyl and under conditions of accelerated thermal oxidation of paraffinic and mineral oils.
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收藏
页码：643 / 646
页数：4
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