Syntheses of imidazo[4,5-e]-1,2,4-triazines via the reaction of 1,3-dimethyl-4,5-dihydroxy-4,5-diphenylimidazolidin-2-one with aminoguanidine and semicarbazide

被引:10
|
作者
Vasilevskii, Sergei V. [1 ]
Nelynbina, Yulia V. [2 ]
Kravchenko, Angelina N. [1 ]
机构
[1] Russian Acad Sci, ND Zelinskii Organ Chem Inst, Moscow 119991, Russia
[2] Russian Acad Sci, AN Nesmeyanov Organoelement Cpds Inst, Moscow 119991, Russia
关键词
DERIVATIVES;
D O I
10.1016/j.mencom.2009.09.017
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
3-Imino-5,7-dimethyl-4a,7a-diphenylperhydroimidazo[4,5-e]-1,2,4-triazin-6-one and 5,7-dimethyl-4a,7a-diphenylperhydroimidazo[4,5-e]-1,2,4-triazine-3,6-dione were synthesized for the first time via the condensation of aminoguanidine and semicarbazide (as hydrochlorides) with 1,3-dimethyl-4,5-dihydroxy-4,5-diphenylimidazolidin-2-one, and a new conglomerate (space group P2(1)) was found by XRD study.
引用
收藏
页码:279 / 280
页数:2
相关论文
共 50 条
  • [1] (4R,5R)-1,3-dimethyl-4,5-diphenylimidazolidin-2-one
    Kawahata, Masatoshi
    Saito, Noriko
    Ishikawa, Tsutomu
    Yamaguchi, Kentaro
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O3488 - O3489
  • [2] Regioselective synthesis of new imidazo[4,5-e][1,3]thiazino[2,3-c][1,2,4]triazines via reaction of imidazo[4,5-e][1,2,4]triazinethiones with ethyl phenylpropiolate
    Vinogradov, Dmitry B.
    Izmest'ev, Alexei N.
    Kravchenko, Angelina N.
    Kolotyrkina, Natalya G.
    Gazieva, Galina A.
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 2024, 61 (01) : 137 - 145
  • [3] SYNTHESES OF SEVERAL PYRIMIDO[4,5-E][1,2,4]TRIAZINES
    SUGIMOTO, T
    MATSUURA, S
    BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1975, 48 (02) : 725 - 726
  • [4] Synthesis of imidazo[4,5-e][1,3]thiazino[2,3-c][1,2,4]triazines via a base-induced rearrangement of functionalized imidazo[4,5-e]thiazolo[2,3-c][1,2,4]triazines
    Vinogradov, Dmitry B.
    Izmest'ev, Alexei N.
    Kravchenko, Angelina N.
    Strelenko, Yuri A.
    Gazieva, Galina A.
    BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY, 2023, 19 : 1047 - 1054
  • [5] Use of tandem AN-AN reactions for the synthesis of thiazolo[4,5-e]-1,2,4-triazines
    Charushin, VN
    Mochulskaya, NN
    Andreiko, AA
    Kodess, MI
    Chupakhin, ON
    MENDELEEV COMMUNICATIONS, 2002, (01) : 28 - 30
  • [6] REACTIVITY OF 4,5-BOND IN 1,2,4-TRIAZINES
    MPACKO, JP
    VINOT, N
    COMPTES RENDUS HEBDOMADAIRES DES SEANCES DE L ACADEMIE DES SCIENCES SERIE C, 1970, 271 (19): : 1201 - &
  • [7] Synthesis of imidazo[4,5-e][1,3]thiazolo-[3,2-b][1,2,4]triazines
    Gazieva, G. A.
    Poluboyarov, P. A.
    Nelyubina, Yu. V.
    Struchkova, M. I.
    Kravchenko, A. N.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2012, 48 (09) : 1382 - 1389
  • [8] Synthesis of imidazo[4,5-e][1,3]thiazolo-[3,2-b][1,2,4]triazines
    G. A. Gazieva
    P. A. Poluboyarov
    Yu. V. Nelyubina
    M. I. Struchkova
    A. N. Kravchenko
    Chemistry of Heterocyclic Compounds, 2012, 48 : 1382 - 1389
  • [9] Synthesis and structure of [1,2]thiaphospholo[4,5-e][1,2,4]triazines
    Ibrahim, YA
    Kadry, AM
    Ibrahim, MR
    Lisgarten, JN
    Potter, BS
    Palmer, RA
    TETRAHEDRON, 1999, 55 (47) : 13457 - 13462
  • [10] Tandem AN-AN reactions in the synthesis of tetrahydrothiazolo[4,5-e][1,2,4]triazines
    Mochulskaya, Nataliya N.
    Slepukhin, Pavel A.
    Charushin, Valery N.
    Kodess, Mikhail I.
    MENDELEEV COMMUNICATIONS, 2016, 26 (05) : 375 - 377