Crystal structure of N,N′-Bis-(2,5-dimethoxybenzylidene)-1,3-diaminopropane

被引：2

作者：

Khalaji, A. D. ^{[1
]}

Fejfarova, K. ^{[2
]}

Dusek, M. ^{[2
]}

机构：

[1] Golestan Univ, Fac Sci, Dept Chem, Gorgan, Iran

[2] ASCR, Inst Phys, Prague 18221 8, Czech Republic

来源：

JOURNAL OF STRUCTURAL CHEMISTRY | 2011年 / 52卷 / 06期

关键词：

X-ray diffraction; orthorhombic symmetry; Schiff base; SCHIFF-BASE;

D O I：

10.1134/S0022476611060175

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The Schiff-base compound N,N'-Bis-(2,5-dimethoxybenzylidene)-1,3-diaminopropan, (2,5-MeO-ba)(2)pn, is synthesized and characterized by elemental analysis, FT-IR and H-1 NMR spectroscopy. The crystal structure of (2,5-MeO-ba)(2)pn is determined by X-ray single crystal diffraction analysis. The X-ray diffraction analysis at 120 K reveals that (2,5-MeO-ba)(2)pn crystallizes in the orthorhombic system, Fdd2 space group with a = 29.339(9) , b = 29.4073(11) , c = 4.4524(2) , V = 3840.8(3) (3), mu = 0.72 mm(-1), and Z = 8.

引用

页码：1131 / 1133

页数：3

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