Determination of herbicides in drinking water by solid phase extraction-liquid chromatography-mass spectrometry

被引:0
|
作者
Ren, J [1 ]
Huang, CL [1 ]
Zhao, GD [1 ]
Jiang, K [1 ]
机构
[1] Chinese Acad Sci, Ecoenvironm Sci Res Ctr, Beijing 100085, Peoples R China
关键词
solid phase extraction-high performance liquid chromatography; solid phase extraction-high performance liquid chromatography-mass spectrometry; drinking water; herbicides; residues;
D O I
暂无
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A method for the determination of micro-herbicides (metsufuron-methyl, simazine, atrazine, simetryn, dimethachior, dipropetryn, propanil) in water has been developed by solid phase extraction-high performance liquid chromatography-mass spectrometry. No special sample pretreatment was applied. It is only need to 45 min to analysis a sample. The detection limit obtained was lower than 0.1 mug/L. This method saves much time in sample preparation than that consumed by liquid-liquid extraction (60 fold) and off-line SPE (20 fold), and is more effective than the other methods. By using this method atrazine (1.9 mug/L) and dimethachlor (1.64 mug/L) have been detected in surface water.
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页码:876 / 880
页数:5
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