Syntheses and structures of mono-, di- and tetranuclear rhodium or iridium complexes of thiacalix[4]arene derivatives

被引：18

作者：

Hirata, K ^{[1
]}

Suzuki, T ^{[1
]}

Noya, A ^{[1
]}

Takei, I ^{[1
]}

Hidai, M ^{[1
]}

机构：

[1] Sci Univ Tokyo, Dept Mat Sci & Technol, Fac Ind Sci & Technol, Noda, Chiba 278, Japan

来源：

CHEMICAL COMMUNICATIONS | 2005年 / 29期

关键词：

D O I：

10.1039/b502999f

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The reactions of [Cp*MCl2](2) (Cp* = eta(5)-C5Me5, M = Rh, Ir) with thiacalix[4]arene (TC4A(OH)(4)) and tetramercaptothiacalix[4] arene (TC4A(SH)(4)) gave the mononuclear complexes [(Cp*M){eta(3)-TC4A(OH)(2)(O)(2)}] and the dinuclear complexes [(Cp*M)(2) {eta(3):eta(3)-TC4A(S)(4)}] respectively, while the analogous reactions with dimercaptothiacalix[4] arene (TC4A(OH)(2)(SH)(2)) produced the tetranuclear complexes [(Cp*M)(2)(Cp*MCl2)(2)-{eta(3):eta(3):eta(1):eta(1)-TC4A(O)(2)(S)(2)}].

引用

页码：3718 / 3720

页数：3

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