Formation of maghemite nanoparticles in bismuth telluride materials containing iron

被引:0
|
作者
Catchings, R. M., III [1 ]
Thorpe, A. N. [1 ]
Grant, J. R. [1 ]
Douglas, R. [1 ]
Viragh, C. [2 ]
Adel-Hadadi, M. A. [3 ]
Gaskell, K. [4 ]
Barkatt, A. [3 ]
机构
[1] Howard Univ, Dept Phys & Astron, Washington, DC 20059 USA
[2] Catholic Univ Amer, Vitreous State Lab, Washington, DC 20064 USA
[3] Catholic Univ Amer, Dept Chem, Washington, DC 20064 USA
[4] Univ Maryland, Dept Chem, College Pk, MD 20742 USA
关键词
TRANSFORMATION; FERRIHYDRITE; HEMATITE; FE3O4; MAGNETITE; BI2TE3;
D O I
10.1557/JMR.2010.0259
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Bismuth telluride (Bi2Te3) systems containing 2%, 4%, and 8% of iron were prepared using a low temperature wet chemical method. Iron oxide nanoparticles were formed when the samples were heated in hydrogen at 250 degrees C for at least six hours. The samples were characterized by x-ray diffraction, magnetization, magnetic susceptibility, x-ray photoelectron spectroscopy, Mossbauer spectroscopy, and wet chemical analysis measurements. The nanoparticles of iron oxide were identified as gamma-Fe2O3 with a particle size of similar to 5 nm.
引用
收藏
页码:2042 / 2046
页数:5
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