Chiral naphthafurophanes from furan macrocycles

被引：3
|
作者：
Fonte, P
Kohnke, FH
Parisi, MF
Menzer, S
Williams, DJ
机构：
[1] UNIV MESSINA,DIPARTIMENTO CHIM ORGAN & BIOL,I-98166 MESSINA,ITALY
[2] UNIV LONDON IMPERIAL COLL SCI TECHNOL & MED,DEPT CHEM,CHEM CRYSTALLOG LAB,LONDON SW7 2AY,ENGLAND
来源：
TETRAHEDRON LETTERS | 1996年 / 37卷 / 34期
关键词：
D O I：
10.1016/0040-4039(96)01324-X
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
The cycloaddition of two moles of benzyne with any two non diametrically opposite furan units of 1 in an anti geometry yields a chiral macrocycle. The chiral anti-1,3-bis-adduct 2 has been isolated, characterised bg X-ray crystallography, and converted into the corresponding dinaphthafuropnane 4. The X-ray analysis of 4 shows the crystals to contain only a single enantiomer i.e. I undergoes spontaneous resolution on crystallisation. Copyright (C) 1996 Elsevier Science Ltd
引用
收藏
页码：6205 / 6208
页数：4
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