Synthesis and characterization of bis-triruthenium cluster derivatives of an all equatorial [60]fullerene tetramalonate

被引：18

作者：

Chen, Chia-Hsiang ^{[1
]}

Aghabali, Amineh ^{[2
]}

Suarez, Catalina ^{[1
]}

Olmstead, Marilyn M. ^{[2
]}

Balch, Alan L. ^{[2
]}

Echegoyen, Luis ^{[1
]}

机构：

[1] Univ Texas El Paso, Dept Chem, El Paso, TX 79968 USA

[2] Univ Calif Davis, Dept Chem, Davis, CA 95616 USA

来源：

CHEMICAL COMMUNICATIONS | 2015年 / 51卷 / 30期

基金：

美国国家科学基金会;

关键词：

FULLERENE; COMPLEXES; C-60; PPH2(O-C6H4)(CH2NMECH)C-60; C-70;

D O I：

10.1039/c4cc10397a

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The reaction of the tetrakis[di(ethoxycarbonyl)methano]-C-60 (1) with Ru-3(CO)(12) afforded the first bis-parallel C-60-metal cluster complex: parallel-[Ru-3(CO)(9)](2){mu(3)-eta(2),eta(2),eta(2)-C-60[C(COOC2H5)(2)](4)}. The two triruthenium groups are found in either a parallel or a tilted orientation relative to each other, as determined by NMR. Only the parallel form was characterized by X-ray crystallography.

引用

页码：6489 / 6492

页数：4

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