Microstructures and mechanical properties of directionally solidified Ni-25%Si full lamellar in situ composites

Directional solidification experiments have been performed on Ni-25 at% Si alloy using electron beam floating zone method. A fully regular eutectic microstructures consisting of Ni, gamma-Ni31Si12 and beta(1)-Ni3Si have been obtained. The influences of the directional solidification rate on the microstructures and properties of the full lamellar structures have been studied. The results show that the relationship between the mean interphase spacing (lambda) and withdrawal rate (v) meets lambda=29.9v(-0.65.) The hardness increases with the increasing of growth rate (v) and decreasing of the interlamellar spacing (lambda) which meets the relationship of H-v=445.2v(0.14) and H-v=910 lambda(-0.21). The maximum compressive strength, 2576 MPa, for DS samples is obtained by 10 mm/h. The average fracture toughness value found for 5 mm/h; 7 mm/h, 10 mm/h is 28.3 MPa m(1/2), 29.1 MPa m(1/2) and 35.9 MPa m(1/2), respectively. The crack bridging and crack deflection/interface debonding are the main toughening mechanism of Ni-25 at Si with full lamellar structures. (C) 2016 Elsevier B.V. All rights reserved.