The application of combinatorial approach in the hydrothermal syntheses of open-framework zinc phosphates

被引：0
|
作者：
Song, Y [1 ]
Yu, J [1 ]
Li, Y [1 ]
Zhang, Y [1 ]
Zhang, M [1 ]
Xu, R [1 ]
机构：
[1] Jilin Univ, State Key Lab Inorgan Synth & Preparat Chem, Changchun 130023, Peoples R China
来源：
RECENT ADVANCES IN THE SCIENCE AND TECHNOLOGY OF ZEOLITES AND RELATED MATERIALS, PTS A - C | 2004年 / 154卷
关键词：
combinatorial approach; zinc phosphates; hydrothermal synthesis; structures;
D O I：
暂无
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
Applying combinatorial approach, new open-framework zinc phosphates have been hydrothermally synthesized in the Zn(OAC)(2)-H3PO4-N, N'-dirnethylpiperazine-H2O system. The experimental design includes variation of the components of the reagents and the crystallization temperature, as well as the study of influence of transition metal cations on the crystallization. Their structures are solved by single-crystal X-ray diffraction analysis, and further characterized by X-ray powder diffraction analysis, ICP, TG and NMR analyses.
引用
收藏
页码：1028 / 1034
页数：7
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