Crystal structure of a novel compound: 1-Phenyl-3-ethyl-4-(salicylidene hydrazide)-propenylidene-pyrazolone-5

被引：0
|
作者：
Chai, H [1 ]
Liu, GF [1 ]
Liu, L [1 ]
Jia, DZ [1 ]
机构：
[1] Xinjiang Univ, Inst Appl Chem, Xinjiang 830046, Peoples R China
来源：
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY | 2005年 / 24卷 / 09期
关键词：
crystal structure; pyrazolone; salicylidene hydrazide;
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A novel compound PMPP-SAL (1-phenyl-3-methyl-4-(salicylidene hydrazide)propenylidene-pyrazolone-5) has been synthesized and characterized by elemental analysis, IR, H-1 NMR and single-crystal X-ray diffraction. The X-ray diffraction reveals that the compound is of orthorhombic, space group Pbca with a = 16.132(5), b = 10.113(3), c = 23.143(7) A, V = 3776(2) A(3), Z = 8, C20H20N4O3, M-r = 364.40, D-c = 1.282 g/cm(3), F(000) = 1536, mu(MoK alpha) = 0.089 mm(-1), S = 0.992, R = 0.0578 and wR = 0.1362 for 1871 observed reflections with I > 2 sigma(I). In the crystal, the compound possesses two C=O bonds and exists in the NH-form' other than NH-form.
引用
收藏
页码：1091 / 1095
页数：5
相关论文
共 50 条
  • [1] Crystal Structure of a Novel Compound: 1-Phenyl-3-ethyl-4-(salicylidene hydrazide)-propenylidene-pyrazolone-5
    柴卉
    刘广飞
    刘浪
    贾殿赠
    Chinese Journal of Structural Chemistry, 2005, (09) : 1091 - 1095
  • [2] Crystal Structure of a Novel Compound: 1-Phenyl-3-ethyl-4-(salicylidene hydrazide)-propenylidene-pyrazolone-5
    柴卉
    刘广飞
    刘浪
    贾殿赠
    结构化学, 2005, (09) : 1091 - 1095
  • [3] Synthesis, Characterization and Crystal Structure of 1-Phenyl-3-methyl-4-(salicylidene hydrazide)-phenylethylene-pyrazolone-5
    Li Zhang
    Guan-Cheng Xu
    Lang Liu
    Guang-Fei Liu
    Dian-Zeng Jia
    Journal of Chemical Crystallography, 2008, 38 : 151 - 155
  • [4] Synthesis, characterization and crystal structure of 1-phenyl-3-methyl-4-(salicylidene hydrazide)-phenylethylene-pyrazolone-5
    Zhang, Li
    Xu, Guan-Cheng
    Liu, Lang
    Liu, Guang-Fei
    Jia, Dian-Zeng
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2008, 38 (02) : 151 - 155
  • [5] The crystal structure of 1-phenyl-3-methyl-4(salicylaldehyde hydrazone)-propenylidene-5-pyrazolone
    Guangfei Liu
    Lang Liu
    Dianzeng Jia
    Kaibei Yu
    Journal of Chemical Crystallography, 2005, 35 : 497 - 501
  • [6] The crystal structure of 1-phenyl-3-methyl-4-(salicylaldehyde hydrazone)-propenylidene-5-pyrazolone
    Liu, GF
    Liu, L
    Jia, DZ
    Yu, JB
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2005, 35 (06) : 497 - 501
  • [7] THEORETICAL STUDIES ON THE CONFORMATION AND COORDINATION OF N-(1-PHENYL-3-METHYL-4-PROPENYLIDENE-5-PYRAZOLONE)-SALICYLIDENE
    Liu, Anjie
    Yang, Yinling
    Jia, Dianzeng
    Wu, Dongling
    Liu, Lang
    Guo, Jixi
    JOURNAL OF THEORETICAL & COMPUTATIONAL CHEMISTRY, 2013, 12 (05):
  • [8] Synthesis and Crystal Structure of N-(1-Phenyl-3methyl-4-benzal-pyrazolone-5)-furoic Hydrazide
    LIU Langa JI Ya-Lia JIA Dian-Zenga② YU Kai-Beib a(Institute of Applied Chemistry
    结构化学, 2003, (05) : 569 - 573
  • [9] Synthesis and crystal structure of N-(1-phenyl-3-methyl-4-benzal-pyrazolone-5)-furoic hydrazide
    Liu, L
    Ji, YL
    Jia, DZ
    Yu, KB
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2003, 22 (05) : 568 - 572
  • [10] Synthesis and crystal structure of N-(1-phenyl-3-methyl-4-benzal-pyrazolone-5)- N′-salicylidene hydrazine
    Lang Liu
    Dianzeng Jia
    Yongmin Qiao
    Yali Ji
    Kaibei Yu
    Journal of Chemical Crystallography, 2002, 32 : 255 - 259
12345