Synthesis, crystal structure and antimicrobial activity of a new ternary mixed ligand complex [Mn(pht)2(phen)]

被引:0
|
作者
Hu Xi-Lan
Xu Xing-You [1 ]
Wang Da-Qi
Xu Tong-Tao
Gu Hai-Xing
机构
[1] Huaihai Inst Technol, Dept Chem Engn, Lianyungang 222005, Jiangsu, Peoples R China
[2] Liaocheng Univ, Coll Chem & Chem Engn, Shandong 252059, Peoples R China
[3] Lianyungang Tech Coll, Dept Chem Engn, Lianyungang 222006, Jiangsu, Peoples R China
关键词
manganese complex; 5,5-diphenylimidazoline-2,4-dione; 1,10-phenanthroline; crystal structure; antimicrobial activity;
D O I
暂无
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
The title complex [Mn(pht)(2)(phen)] (Hpht=5,5-diphenylimidazoline-2,4-dione, phen=1,10-phenanthroline) was synthesized and characterized by elemental analysis, IR and X-ray diffraction single-crystal structure analysis. The compound crystallizes in the monoclinic system, space group C2/c with a=2.631 5(16) nm, b=0.9245(6) nm, c= 1.5508(10) nm, beta=116.231(7)degrees; V=3.384(4) nm(3), M-x=737.66, Z=4, F(000)= 1524, D-c= 1.448 g.cm(-3), mu=0.446 mm(-1), the final R=0.0699 and wR=0.195 3. The complex was valued for its antimicrobial activity against so-me bacteria in vitro. It was found to be active against the four test bacterial organisms. CCDC: 616309.
引用
收藏
页码:1675 / 1678
页数:4
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