Preparation of c-axis oriented YBa2Cu3O7 polycrystalline ceramics by sol-gel method

被引:3
|
作者
Wang, Wenzhang [1 ]
Chen, Qingming [1 ]
Cui, Qi [1 ]
Ma, Ji [1 ]
Zhang, Hui [1 ]
机构
[1] Kunming Univ Sci & Technol, Fac Mat Sci & Engn, Kunming 650093, Peoples R China
基金
美国国家科学基金会;
关键词
YBa2Cu3O7; Sol-gel; c-axis preferred orientation; SUPERCONDUCTORS;
D O I
10.1016/j.physc.2015.02.003
中图分类号
O59 [应用物理学];
学科分类号
摘要
YBa2Cu3O7 powders and ceramics with c-axis preferred orientation were synthesized by sol-gel method. The pure phase powders were obtained when calcined between 800 and 930 degrees C, and the ceramics were sintered at 950 degrees C. It was found that c-axis orientated ceramics were obtained only when the powders were calcined at 930 degrees C. The X-ray diffraction patterns show that the relative intensities of c-axis (00l) peaks are much stronger than that of the standard pattern. The surface morphology own an obvious layered structure and the grains are platelike grown. The transition temperature T-C(onset) is 93.67 K with a transition width Delta T-c of 2.1 K. (C) 2015 Elsevier B.V. All rights reserved.
引用
收藏
页码:1 / 3
页数:3
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