Bis{(E)-N′-[2,4-bis(trifluoromethyl)benzylidene]isonicotinohydrazide} monohydrate

被引：3

作者：

Naveenkumar, H. S. ^{[2
]}

Sadikun, Amirin ^{[2
]}

Ibrahim, Pazilah ^{[2
]}

Yeap, Chin Sing ^{[1
]}

Fun, Hoong-Kun ^{[1
]}

机构：

[1] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, Usm 11800, Penang, Malaysia

[2] Univ Sains Malaysia, Sch Pharmaceut Sci, Usm 11800, Penang, Malaysia

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷

关键词：

D O I：

10.1107/S1600536810025493

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The asymmetric unit of the title compound, 2C(15)H(9)F(6)N(3)O center dot H2O, contains two independent Schiff base molecules and one water molecule. Both Schiff base molecules exist in an E configuration with respect to the C=N double bonds and the dihedral angles between the benzene and the pyridine rings in the two molecules are 17.53 (12) and 20.62 (12)degrees. In the crystal structure, molecules are linked by intermolecular N-H...O and C-H...O hydrogen bonds into infinite one-dimensional chains along the a axis. In addition, intermolecular O-H...N, O-H...F, C-H...F and C-H...O hydrogen bonds further link these chains into a three-dimensional network. Weak pi-pi interactions with centroid-centroid distances in the range 3.6495 (17)-3.7092 (16) A are also observed.

引用

页码：O1918 / U346

页数：14

共 50 条

[1] PREPARATION OF BIS[2,4-BIS(TRIFLUOROMETHYL)PHENYL]FLUOROPHOSPHINE AND 2,4-BIS(TRIFLUOROMETHYL) PHENYL-[2,6-BIS(TRIFLUOROMETHYL)PHENYL]-FLUOROPHOSPHINE - 2 DISTILLABLE MONOFLUOROPHOSPHINES - STRUCTURE OF CIS-DICHLORO-BIS[BIS(2,4-BIS(TRIFLUOROMETHYL)PHENYL)FLUOROPHOSPHINO]-PLATINUM(II)
HEUER, L
JONES, PG
SCHMUTZLER, R
JOURNAL OF FLUORINE CHEMISTRY, 1990, 46 (02) : 243 - 254
[2] A convenient, selective synthesis of bis[2,4-bis(trifluoromethyl)phenyl]phosphane - Derivatives starting from 1,3-bis(trifluoromethyl)benzene
Hoge, Berthold
Kurscheid, Boris
Peuker, Sebastian
Tyrra, Wieland
Fischer, Hendrik T. M.
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2007, 633 (10): : 1679 - 1685
[3] Application of 2,4-bis(halomethyl)quinoline: synthesis and biological activities of 2,4-bis(benzofuran-2-yl)- and 2,4-bis(aroxymethyl)quinolines
Yang Li
Qiqi Xu
Zhiyuan Li
Wentao Gao
Yu Chen
Molecular Diversity, 2020, 24 : 167 - 178
[4] Application of 2,4-bis(halomethyl)quinoline: synthesis and biological activities of 2,4-bis(benzofuran-2-yl)- and 2,4-bis(aroxymethyl)quinolines
Li, Yang
Xu, Qiqi
Li, Zhiyuan
Gao, Wentao
Chen, Yu
MOLECULAR DIVERSITY, 2020, 24 (01) : 167 - 178
[5] Tetrakis[2,4-bis(trifluoromethyl)phenyl]diphosphoxane: An anhydride of a phosphinous acid
Hoge, Berthold
Kurscheid, Boris
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2008, 47 (36) : 6814 - 6816
[6] 2,4-BIS(BROMOMETHYL)-5-METHYL-N-ACETYL BENZYLAMINE AND 2,4-BIS(CYANOMETHYL)-5-METHYL-N-ACETYLBENZYLAMINE
KUNDU, NG
PECK, J
EVANGELATOS, DW
ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 1982, 14 (03) : 206 - 208
[7] 2,4-Bis(α,α-dimethylbenzyl)phenol
Bryan, Jeffrey C.
Acta Crystallographica, Section C: Crystal Structure Communications, 2000, 56 (08) : 1046 - 1047
[8] 2,4-Bis(α,α-dimethylbenzyl)phenol
Bryan, JC
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2000, 56 : 1046 - 1047
[9] NEW DIAZADIPHOSPHETIDINE COMPLEXES - (2,4-BIS(DIMETHYLAMINO)-1,3-BIS(TRIMETHYLSILYL)-1,3,2,4-DIAZADIPHOSPHETIDINE)-2,4-BIS(PENTACARBONYLCHROMIUM) AND (2,4-BIS(DIMETHYLAMINO)-1,3-BIS(TRIMETHYLSILYL)-1,3,2,4-DIAZADIPHOSPHETIDINE)-2,4-BIS(PENTACARBONYLMOLYBDENUM)
ZEISS, W
FELDT, C
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1977, 127 (01) : C5 - C8
[10] 2,4-Bis[2-chloro-4-(trifluoromethyl)phenoxy]-1-nitrobenzene
Gao, S
Ng, SW
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O3763 - O3764

← 1 2 3 4 5 →