An Alternative Synthesis of 2,6-Dimethoxyl-1,4-Benzoquinone

被引：1

作者：

Wang, Qian ^{[1
]}

Yang, Jian ^{[1
]}

Zheng, Yang ^{[1
]}

Liao, Xiali ^{[1
]}

机构：

[1] Kunming Univ Sci & Technol, Fac Life Sci & Technol, 727 South Jingming Rd, Kunming 650500, Yunnan, Peoples R China

来源：

JOURNAL OF CHEMICAL RESEARCH | 2017年 / 41卷 / 04期

基金：

中国国家自然科学基金;

关键词：

2; 6-dimethoxy-1; 4-benzoquinone; aniline;

D O I：

10.3184/174751917X14894997017379

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

An economic four-step synthesis of 2,6-dimethoxy-1,4-benzoquinone was achieved in 68% overall yield starting from aniline. The reaction sequence involved conversion to 1,3,5-tribromoaniline, deamination, methoxylation, and oxidation. The procedure is operationally simple and amenable to scale-up production.

引用

页码：193 / 194

页数：2

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