A Simple, Inexpensive, Mercury-Free Bubbler Apparatus

被引:1
|
作者
Johnson, Sara E. [1 ]
West, Joseph K. [1 ]
机构
[1] Winona State Univ, Dept Chem, Winona, MN 55987 USA
关键词
Laboratory Equipment/Apparatus; Inorganic Chemistry; Organometallics; Upper-Division Undergraduate; Safety/Hazards; Hands-On Learning/Manipulatives; Laboratory Instruction; SCHLENK LINE; SYNTHETIC EXPERIMENTS; CHEMISTRY; MANIPULATION; CANNULA; COMPLEX; ALKYNE;
D O I
10.1021/acs.jchemed.1c00224
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Inert gas manifolds for the handling of air-sensitive materials are commonplace in the inorganic chemistry curriculum as well as in research laboratories specializing in inorganic and organometallic synthesis. Mercury bubblers are ubiquitously implemented for maintaining a positive internal pressure for air-free manifold systems, commonly known as Schlenk lines. This has rendered them difficult to replace with equivalent and accessible alternatives. This communication describes the setup and implementation of a simple, inexpensive alternative to the traditional mercury bubbler that is modular and flexible enough to fit most any laboratory space.
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收藏
页码:2482 / 2485
页数:4
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