Asymmetric Addition Reaction Catalyzed by 1-(2-Hydroxynaphthalen-1-yl)naphthalen-2-ol Functionalized Porous Organic Polymer

被引：2
|
作者：
Kong, Shengnan [1 ]
Qian, Xuefeng [1 ]
Shu, Mouhai [1 ]
Xiao, Wende [1 ]
机构：
[1] Shanghai Jiao Tong Univ, Sch Chem & Chem Engn, Shanghai 200240, Peoples R China
来源：
CHINESE JOURNAL OF ORGANIC CHEMISTRY | 2018年 / 38卷 / 10期
基金：
中国国家自然科学基金;
关键词：
porous organic polymers; BINOL; heterogeneous catalysis; asymmetric addition reaction; CONJUGATED MICROPOROUS POLYMERS; CROSS-LINKED POLYMERS; INTRINSIC MICROPOROSITY; CARBONYL-ENE; FRAMEWORKS; REDUCTION; NETWORKS; DIETHYLZINC; ADSORPTION;
D O I：
10.6023/cjoc201804011
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A functionalized porous organic polymer POP-BINOL has been prepared and characterized by various techniques including carbon-13 cross-polarization magic-angle spinning nuclear magnetic resonance (C-13 CP/MAS NMR), fourier transform infrared spectroscopy (FT-IR), powder X-ray diffraction (pXRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), nitrogen adsorption and thermogravimetric analysis (TG). After being treated with Ti(OiPr)(4), the composite material could be used as highly effective and reusable heterogeneous catalyst for asymmetric diethylzinc addition to aldehydes with medium and upper ee value.
引用
收藏
页码：2754 / 2760
页数：7
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