Synthesis of semiaromatic polyimides from aromatic diamines containing adamantyl units and alicyclic dianhydrides

被引：56

作者：

Watanabe, Y ^{[1
]}

Shibasaki, Y ^{[1
]}

Ando, S ^{[1
]}

Ueda, M ^{[1
]}

机构：

[1] Tokyo Inst Technol, Grad Sch Sci & Engn, Dept Organ & Polymer Mat, Meguro Ku, Tokyo 1528552, Japan

来源：

JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY | 2004年 / 42卷 / 01期

关键词：

adamantane; biadamantane; polyimides; thermal properties; refractive index;

D O I：

10.1002/pola.10990

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

We prepared new semiaromatic polyimides from alicyclic dianhydrides and aromatic diamines containing adamantyl and biadamantyl units. Polycondensations were performed in 1-methyl-2-pyrrolidinone at room temperature for 7 h and then 80 degreesC for 23 h, giving poly(amic acid)s with inherent viscosities up to 0.58 dL/g. Poly(amic acid)s were converted to corresponding poly(imide)s by thermal treatment. Poly(imide)s showed relatively high thermal stability (5% weight loss around 450 degreesC) and low dielectric constants (2.69-2.79). (C) 2003 Wiley Periodicals, Inc.

引用

页码：144 / 150

页数：7

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