Identification of antioxidant phenolic. compounds in feverfew (Tanacetum parthenium) by HPLC-ESI-MS/MS and NMR

被引：36
|
作者：
Wu, Changqing [1 ]
Chen, Feng
Wang, X.
Wu, Yonnie
Dong, Meidui
He, Guoqing
Galyean, Ronald D.
He, Lilin
Huang, Guohui
机构：
[1] Clemson Univ, Dept Food Sci & Human Nutr, Clemson, SC 29634 USA
[2] Clemson Univ, Dep Genet Chem, Clemson, SC 29634 USA
[3] Clemson Univ, Dept Agr & Biol Engn, Clemson, SC 29634 USA
[4] Zhejiong Univ, Dept Food Sci & Nutr, Hangzhou 310029, Peoples R China
[5] Clemson Univ, Dept Chem, Clemson, SC 29634 USA
来源：
PHYTOCHEMICAL ANALYSIS | 2007年 / 18卷 / 05期
关键词：
feverfew; LC-MS; NMR; phenolics; dicaffeoylquinic acid; antioxidant;
D O I：
10.1002/pca.995
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
Antioxidant polyphenolic acids in the medicinal herb feverfew (Tanacetum parthenium) were isolated through in vitro bioassay-orientated antioxidant tests in response to 1,1-diphenyl-2-picrylhydrazyl (DPPH center dot) free radical scavenging and Fe2+-chelating activities. Purification of the active compounds and their structural elucidation involved a variety of techniques including open-column chromatography, HPLC, GC-MS, LC-MS and NMR. Major compounds with potent DPPH center dot scavenging activities were characterised as 3,5-, 4,5- and 3,4-di-O-caffeoylquinic acids (DCQAs). This is the first report of DCQAs found in feverfew. Copyright (c) 2007 John Wiley & Sons, Ltd.
引用
收藏
页码：401 / 410
页数：10
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