Microwave Assisted Synthesis of Highly Luminescent ZnS Nanostructures Using Zinc Dithiocarbazic Complex Chemical Route

被引：1

作者：

Sharma, Ranjana ^{[1
]}

Singh, Bhoop ^{[1
]}

Kumar, Vijay ^{[2
]}

Goswami, Y. C. ^{[2
]}

Singh, Rajeev ^{[1
]}

Kumar, D. ^{[3
]}

机构：

[1] ITM GOI, Dept Chem & Environm Sci, Gwalior 474001, MP, India

[2] ITM Univ, Sch Phys Sci, Gwalior 474001, MP, India

[3] SMS Govt Sci Coll, PG Dept Chem, Gwalior 474001, MP, India

来源：

ADVANCES IN OPTICAL SCIENCE AND ENGINEERING | 2015年 / 166卷

关键词：

NANOWIRES;

D O I：

10.1007/978-81-322-2367-2_71

中图分类号：

O43 [光学];

学科分类号：

070207 ; 0803 ;

摘要：

Bis(parahydroxyacetophenonebenzyldithiocarbazate) zinc(II) and bis (acetophenonebenzyldithiocarbazate) zinc(II) complexes have been synthesized. Zinc sulphide nanostructures were obtained from both complexes at different deposition temperatures using microwave assisted chemical route. The surface morphology of as-prepared ZnS nanoparticles were obtained using X-ray diffraction (XRD), transmission electron microscopy (TEM) and high transmission electron microscopy (HRTEM). Particles with spherical shape are shown in the TEM images of these samples. The optical properties of the particles studied by UV-Vis and photoluminescence (PL) spectroscopy showed evidence of quantum confinement.

引用

页码：575 / 580

页数：6

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