Combustion assisted synthesis of hardystonite nanopowder

被引：28

作者：

Sadeghzade, Sorour ^{[1
]}

Emadi, Rahmatollah ^{[1
]}

Tavangarian, Fariborz ^{[2
]}

机构：

[1] Isfahan Univ Technol, Dept Mat Engn, Biomat Res Grp, Esfahan 8415683111, Iran

[2] Penn State Harrisburg, Sch Sci Engn & Technol, Mech Engn Program, Middletown, PA 17057 USA

来源：

CERAMICS INTERNATIONAL | 2016年 / 42卷 / 13期

关键词：

Sintering; X-ray methods; Biomedical applications; LUMINESCENCE; POWDERS; ZINC;

D O I：

10.1016/j.ceramint.2016.06.088

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

In this study, single-phase hardystonite (Ca2ZnSi2O6) nanopowder was synthesized by combustion synthesis method from aqueous solution of Calcium nitrate, Zinc nitrate and Tetraethyl orthosilicate. In order to characterize the obtained powders, X-ray diffraction (XRD), transmission electron microscopy (TEM) and scanning electron microscopy (SEM) were used. The effect of sucrose concentration on the purity and morphology of the obtained hardystonite powder, and its initial annealing temperature was investigated. The optimum sucrose to metal ratio was found to be 2:1. The average particle size and the maximum crystallite size of the produced hardystonite nanopowder were 220 and 40 nm, respectively. (C) 2016 Elsevier Ltd and Techna Group S.r.l. All rights reserved.

引用

页码：14656 / 14660

页数：5

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