Synthesis and Characterization of Nano-γ-Fe2O3 by Sol-Gel Method

被引：0
|
作者：
Huang, Jian [1 ]
Gong, Zhuqing [2 ]
Yang, Xiyun [2 ]
机构：
[1] Cent S Univ, Coll Chem & Chem Engn, Changsha 410083, Peoples R China
[2] Cent S Univ, Coll Met Sci & Engn, Changsha 410083, Peoples R China
来源：
ADVANCED SCIENCE LETTERS | 2011年 / 4卷 / 11-12期
基金：
中国国家自然科学基金;
关键词：
Nano-gamma-Fe2O3; Sol-Gel; Ferric Citrate; Magnetic Material; DUAL-COLOR HYBRIDIZATION; IRON-OXIDE NANOPARTICLES; SINGLE-BASE EXTENSION; MAGNETIC NANOPARTICLES; GAMMA-FE2O3; NANOPARTICLES; IMMUNOLOGICAL METHOD; ARRAY; FABRICATION; SURFACE; ROUTE;
D O I：
10.1166/asl.2011.1864
中图分类号：
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号：
07 ; 0710 ; 09 ;
摘要：
The synthesis and characterization of nano-gamma-Fe2O3 was described by sol-gel method. The optimal conditions for the formation of iron citric acid sol-gel were that the concentration of ferrite citrate was 0.8 mol/L, the pH was 7 and the reaction temperature was 40 degrees C. DTA, XRD, FT-IR, and TEM analysis were employed to characterize the properties of the as-prepared gamma-Fe2O3. TG-DTA, XRD and FT-IR characterization indicate that the appropriate temperature for the formation of gamma-Fe2O3 by Sol-gel method is 450 degrees C and the particle size of gamma-Fe2O3 formed is about 32 nm by the Scherrer formula and TEM under the optimal conditions.
引用
收藏
页码：3662 / 3665
页数：4
相关论文
共 50 条
  • [1] Synthesis and Characterization of Fe2O3 Prepared Via Sol-Gel Method
    Rahman, Noor Azreen Abdul
    Mustaffa, Nur Amalina
    Aziz, Nor Diyana Abdul
    Bader, Nurhanna
    Kannarulzaman, Norlida
    ADVANCEMENT OF MATERIALS AND NANOTECHNOLOGY II, 2012, 545 : 410 - 413
  • [2] Sol-gel synthesis and characterization of α-Fe2O3 nanoparticles
    Raja, K.
    Jaculine, M. Mary
    Jose, M.
    Verma, Sunil
    Prince, A. A. M.
    Ilangovan, K.
    Sethusankar, K.
    Das, S. Jerome
    SUPERLATTICES AND MICROSTRUCTURES, 2015, 86 : 306 - 312
  • [3] Preparation and characterization of α-FeOOH and α-Fe2O3 by sol-gel method
    Dar, MA
    Kulkarni, SK
    Ansari, ZA
    Ansari, SG
    Shin, HS
    JOURNAL OF MATERIALS SCIENCE, 2005, 40 (11) : 3031 - 3034
  • [4] Synthesis, characterization and magnetic properties of ε-Fe2O3 nanoparticles prepared by sol-gel method
    Khan, Irfan
    Morishita, Sakura
    Higashinaka, Ryuji
    Matsuda, Tatsuma D.
    Aoki, Yuji
    Kuzmann, Erno
    Homonnay, Zoltan
    Katalin, Sinko
    Pavic, Luka
    Kubuki, Shiro
    JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2021, 538
  • [5] Nanometric particle size and phase controlled synthesis and characterization of γ-Fe2O3 or (α + γ)-Fe2O3 by a modified sol-gel method
    Silva, M.F. (celafs@gmail.com), 1600, American Institute of Physics Inc. (114):
  • [6] Growth of nano-α-Fe2O3 in a titania matrix by the sol gel route
    Kundu, TK
    Mukherjee, M
    Chakravorty, D
    Sinha, TP
    JOURNAL OF MATERIALS SCIENCE, 1998, 33 (07) : 1759 - 1763
  • [7] Growth of nano-α-Fe2O3 in a titania matrix by the sol–gel route
    T. K Kundu
    M Mukherjee
    D Chakravorty
    T. P Sinha
    Journal of Materials Science, 1998, 33 : 1759 - 1763
  • [8] Sol-gel mediated synthesis of Fe2O3 nanorods
    Woo, K
    Lee, HJ
    Ahn, JP
    Park, YS
    ADVANCED MATERIALS, 2003, 15 (20) : 1761 - +
  • [9] Nanometric particle size and phase controlled synthesis and characterization of γ-Fe2O3 or (α plus γ)-Fe2O3 by a modified sol-gel method
    Silva, Marcela F.
    de Oliveira, Luiz A. S.
    Ciciliati, Mariani A.
    Silva, Lais T.
    Pereira, Bruna S.
    Hechenleitner, Ana Adelina W.
    Oliveira, Daniela M. F.
    Pirota, Kleber R.
    Ivashita, Flavio F.
    Paesano, Andrea, Jr.
    Martin Pastor, J.
    Inaki Perez-Landazabal, J.
    Pineda, Edgardo A. G.
    JOURNAL OF APPLIED PHYSICS, 2013, 114 (10)
  • [10] Synthesis and characterization of Y2O3/Fe2O3/TiO2 nanoparticles by sol-gel method
    Ismail, AA
    APPLIED CATALYSIS B-ENVIRONMENTAL, 2005, 58 (1-2) : 115 - 121
12345