Synthesis of novel molecular clips based on diethoxycarbonyl glycoluril

被引：37
|
作者：
Yin, GD [1 ]
Wang, ZG
Chen, YF
Wu, AX
Pan, YJ
机构：
[1] Cent China Normal Univ, Key Lab Pesticide & Chem Biol, Minist Educ, Wuhan 430079, Peoples R China
[2] Zhejiang Univ, Dept Chem, Hangzhou 310027, Peoples R China
来源：
SYNLETT | 2006年 / 01期
关键词：
molecular clips; diethoxycarbonyl glycoluril; aromatic amines; synthetic receptors; conformers;
D O I：
10.1055/s-2005-922761
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A novel class of molecular clips was synthesized I which are soluble in most non-polar organic solvents. Aromatic amines and diethoxycarbonyl glycoluril were used for the first time in this type of reaction. All reaction products gave satisfying H-1 NMR, C-13 NMR, MS, and IR spectra. In addition, the structure and conformation of 4d were confirmed by single crystal X-ray diffraction.
引用
收藏
页码：49 / 52
页数：4
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