Matrix Solid Phase Dispersion Coupled with Ultra-Fast Liquid Chromatography for Detection of Sulfonamides in Beef Tissue

被引：9

作者：

Wang Chong-Yang ^{[1
]}

Wang Yuan-Peng ^{[1
]}

Wang Ning ^{[2
]}

Jiang Chun-Zhu ^{[1
]}

Yu Xi ^{[1
]}

Song Da-Qian ^{[1
]}

Sun Ying ^{[1
]}

机构：

[1] Jilin Univ, Coll Chem, Changchun 130012, Peoples R China

[2] Jilin Prov Peoples Hosp, Dept Med Sci & Educ, Changchun 130022, Peoples R China

来源：

CHINESE JOURNAL OF ANALYTICAL CHEMISTRY | 2013年 / 41卷 / 01期

关键词：

Matrix solid phase dispersion; Ultra-fast liquid chromatography; Sulfonamides; Beef; MASS-SPECTROMETRY; EXTRACTION; RESIDUES; MEAT; PORK;

D O I：

10.3724/SP.J.1096.2013.20535

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The matrix solid phase dispersion (MSPD) coupled with ultra. fast liquid chromatography (UFLC) was applied for the simultaneous determination of sulfonamides, including sulfathiazole (ST), sulfamerazine (SM1), sulfamethoxazole (SMZ) and sulfadimethoxine (SDM) in beef tissue. The optimized conditions for MSPD and UFLC were as follows: kieselguhr was used as dispersant, 6 mL methanol was used as elution solvent and the mass ratio of sample to dispersant was 1:4. Limits of detection and quantifications of the analytes were 4.39-7.82 ng/g and 14.62-26.08 ng/g, respectively. The spiked samples were analyzed and the recoveries of ST, SM1, SMZ and SDM were 71.73%-113.13%. RSD values were 1.9%-12.4%.

引用

页码：83 / 87

页数：5

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