A self-propagating high-temperature synthesis method for synthesis of zinc oxide powder

被引：13

作者：

Hwang, Chyi-Ching ^{[1
]}

Lin, Cheng-Shiung ^{[2
]}

Wang, Gaw-Pying ^{[3
]}

Peng, Cheng-Hsiung ^{[4
]}

Chung, Shyan-Lung ^{[5
]}

机构：

[1] Chung Cheng Inst Technol, Dept Appl Chem & Mat Sci, NDU, Tao Yuan 33509, Taiwan

[2] Chung Cheng Inst Technol, Sch Def Sci, NDU, Tao Yuan 33509, Taiwan

[3] Chung Shan Inst Sci & Technol, Chem Syst Res Div, Tao Yuan 325, Taiwan

[4] Ming Hsin Univ Sci & Technol, Dept Mat Sci & Engn, Hsinchu 304, Taiwan

[5] Natl Cheng Kung Univ, Dept Chem Engn, Tainan 70101, Taiwan

来源：

JOURNAL OF ALLOYS AND COMPOUNDS | 2009年 / 467卷 / 1-2期

关键词：

SHS; ZnO; Tetrapod; Morphology; Reaction mechanism; COMBUSTION SYNTHESIS; OPTICAL-PROPERTIES; ZNO POWDERS; PHOTOLUMINESCENCE; CRYSTALS; NITRATE; GROWTH; ARRAYS;

D O I：

10.1016/j.jallcom.2007.12.088

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

A self-propagating high-temperature synthesis (SHS) method has been developed for synthesis of ZnO powder. Powders of Zn and an appropriate amount of NH(4)NO(3) were mixed and pressed into a compact place in a closed chamber with air atmosphere. The combustion reaction was ignited by heating the reactant compact directly using nichrome coil, and then as-synthesized products mainly composed of tetrapod whiskers could be obtained. Both the reaction phenomenon and the product yield were affected by the reactant composition and the stacking density, which might be explained by a proposed reaction mechanism. (C) 2008 Elsevier B.V. All rights reserved.

引用

页码：514 / 523

页数：10

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