Turning DSC Charts of Polymorphs into Phase Diagrams: A Tutorial Paper

被引:26
|
作者
Threlfall, Terence L. [1 ]
机构
[1] Univ Southampton, Sch Chem, Southampton SO17 1BJ, Hants, England
关键词
PHYSICOCHEMICAL PROPERTIES; SOLUBILITY; PHARMACEUTICALS; SULFATHIAZOLE; TEMPERATURE; CALORIMETRY; FORMS;
D O I
10.1021/op900158a
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
A DSC chart can be turned into a phase diagram generally only with the aid of other experimental information, such as solubility measurements or slurrying experiments. There are several ways of presenting phase behaviour diagrammatically. It is shown how to produce a phase diagram and how to avoid some of the potential errors of the experimental measurements.
引用
收藏
页码:1224 / 1230
页数:7
相关论文
共 32 条
  • [1] A MULTIMEDIA TUTORIAL ON PHASE-EQUILIBRIA DIAGRAMS
    BEGLEY, EF
    LINDSAY, CG
    AMERICAN CERAMIC SOCIETY BULLETIN, 1993, 72 (12): : 103 - 104
  • [2] DETERMINATION OF ORGANIC-PHASE DIAGRAMS BY THE DSC METHOD
    RADOMSKI, R
    JOURNAL OF CRYSTAL GROWTH, 1983, 65 (1-3) : 509 - 510
  • [3] Adjoining phase regions on two-dimensional phase diagrams: A tutorial
    Raghavan, V
    Antia, DP
    JOURNAL OF PHASE EQUILIBRIA, 2000, 21 (02): : 121 - 124
  • [4] Ab initio calculations of surface phase diagrams of silica polymorphs
    Chagarov, E
    Demkov, AA
    Adams, JB
    PHYSICAL REVIEW B, 2005, 71 (07):
  • [5] Guiding Synthesis of Polymorphs of Materials Using Nanometric Phase Diagrams
    Ma, Xuetian
    Nolan, Adelaide M.
    Zhang, Shuo
    Bai, Jianming
    Xu, Wenqian
    Wu, Lijun
    Mo, Yifei
    Chen, Hailong
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2018, 140 (49) : 17290 - 17296
  • [6] APPLICATION OF SIMULTANEOUS THERMOMICROSCOPY DSC TO THE STUDY OF PHASE-DIAGRAMS
    WIEDEMANN, HG
    BAYER, G
    JOURNAL OF THERMAL ANALYSIS, 1985, 30 (06): : 1273 - 1281
  • [7] DSC study and phase diagrams calculation of binary systems of paracetamol
    Klimova, K.
    Leitner, J.
    THERMOCHIMICA ACTA, 2012, 550 : 59 - 64
  • [8] APPLICATION OF SIMULTANEOUS THERMOMICROSCOPY/DSC TO THE STUDY OF PHASE DIAGRAMS.
    Wiedemann, H.G.
    Bayer, G.
    Journal of thermal analysis, 1984, 30 (06): : 1273 - 1281
  • [9] Are Crystal Phase Diagrams Predictable with Force Fields? Case of Benzene Polymorphs
    Hofmann, D. W. M.
    Kuleshova, L. N.
    CRYSTAL GROWTH & DESIGN, 2014, 14 (08) : 3929 - 3934
  • [10] REPRESENTATION OF THE DIFFERENT TYPES OF PHASE-DIAGRAMS OF A MULTICOMPONENT SYSTEM BY PHASE FRACTION CHARTS
    DESHPANDE, NU
    NAIK, BY
    GADGEEL, VL
    SCRIPTA METALLURGICA, 1989, 23 (06): : 855 - 858