Chemical reduction synthesis of hexagonal B-C-N compound

被引：2
|
作者：
Sun Guang [1 ]
Wu Qing-Hua [1 ]
Hu Qian-Ku [1 ]
Yu Dong-Li [2 ]
机构：
[1] Henan Polytech Univ, Inst Mat Sci & Engn, Jiaozuo 454000, Peoples R China
[2] Yanshan Univ, State Key Lab Metastable Mat Sci & Technol, Qinhuangdao 066004, Peoples R China
来源：
JOURNAL OF INORGANIC MATERIALS | 2008年 / 23卷 / 05期
关键词：
hexagonal B-C-N compound; chemical reduction synthesis method; X-ray diffraction; electron energy loss spectroscopy;
D O I：
10.3724/SP.J.1077.2008.01067
中图分类号：
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
Hexagonal B-C-N compounds were successfully synthesized by using hydrogen-free 1,3,5-trichlorotriazine and boron tribromide as reactants and metal sodium as reluctant through a chemical reduction synthesis method at 450 degrees C. The synthesized sample was characterized by X-ray diffraction (XRD), transmission electron microscope (TEM), selected area electron diffraction (SAED), electron energy loss spectroscope (EELS) and Fourier transformation infrared spectroscope (FTIR), respectively. The results indicate that the synthesized B-C-N compound is polycrystalline with hexagonal structure and its composition is B0.5C0.07N0.43.
引用
收藏
页码：1067 / 1069
页数：3
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