Uniaxial negative thermal expansion in crystals of tienoxolol

被引：21
|
作者：
Nicolai, Beatrice [1 ]
Rietveld, Ivo B. [1 ]
Barrio, Maria [2 ]
Mahe, Nathalie [1 ]
Tamarit, Josep-Lluis [2 ]
Ceolin, Rene [1 ]
Guechot, Christophe [3 ]
Teulon, Jean-Marie
机构：
[1] Univ Paris 05, Fac Pharm, EAD Physicochim Ind Medicament EA4066, Chim Phys Lab, F-75006 Paris, France
[2] Univ Politecn Cataluna, Dept Fis & Engn Nucl, GCM, ETSEIB, E-08028 Barcelona, Spain
[3] Solvay SA, F-75009 Paris, France
来源：
STRUCTURAL CHEMISTRY | 2013年 / 24卷 / 01期
关键词：
Drug; Active pharmaceutical ingredient (API); Crystal structure; Solid state; HYDROGEN-BOND PATTERNS; POLYMORPHISM; TENSOR; TEMPERATURE; ORIGIN; ZRW2O8;
D O I：
10.1007/s11224-012-0078-z
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The thermal expansion of tienoxolol has been investigated by X-ray powder diffraction up to its melting temperature. The data indicate that the expansion is anisotropic and even negative in one direction of the unit cell. The supramolecular structure formed by hydrogen-bonds reflects that of a trellis, which explains the observed behavior of tienoxolol crystals.
引用
收藏
页码：279 / 283
页数：5
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