Template-free mesoporous LTA zeolite synthesized using microwave heating in the flow system

被引：6
|
作者：
Nagase, Takako [1 ]
Miyakawa, Masato [1 ]
Nishioka, Masateru [1 ]
机构：
[1] Natl Inst Adv Ind Sci & Technol, Miyagino Ku, 4-2-1 Nigatake, Sendai, Miyagi 9838551, Japan
来源：
MICROPOROUS AND MESOPOROUS MATERIALS | 2020年 / 306卷
关键词：
Microwave flow system; Mesoporous LTA zeolite; Template-free; Crystal-grains; Magnetic field; CRYSTALS;
D O I：
10.1016/j.micromeso.2020.110375
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
Mesoporous LTA zeolite was synthesized by heating only the organic-free mother slurry that runs through a flow-type microwave reactor system within a few minutes. The synthesized LTA particles were well-crystallized automorphic crystals with a diameter range of 300-600 nm. Each particle consisted of small crystal-grains, which exhibited a mesopomus feature. The vapor adsorption characteristics confirmed that water adsorption occurs in the mesopomus region in addition to adsorption in the micropores.
引用
收藏
页数：5
相关论文
共 50 条
  • [1] ACTIVATION OF TEMPLATE-FREE SYNTHESIZED PENTASIL ZEOLITE CATALYSTS
    BECKER, K
    BERROUSCHOT, D
    KRAAK, P
    SCHODEL, R
    SCHWIEGER, W
    CHEMIE INGENIEUR TECHNIK, 1992, 64 (11) : 1026 - 1028
  • [2] Phi zeolite synthesized by template-free method for selective catalytic reduction of NO
    Yang R.
    Yu L.
    Zhao X.
    Yang X.
    Gao Z.
    Fu G.
    Jiang J.
    Lian W.
    Liu W.
    Fan Q.
    Huagong Xuebao/CIESC Journal, 2020, 71 (12): : 5578 - 5588
  • [3] Synthesis of Mesoporous LTA Zeolite with Bridged Silsesquioxane as Template
    Liu, Hong-Tao
    Song, Guo-Qiang
    Meng, Ying
    Li, Fu-Xiang
    ASIAN JOURNAL OF CHEMISTRY, 2014, 26 (13) : 3927 - 3931
  • [4] Preparation of Si-rich LTA zeolite membrane using organic template-free solution for methanol dehydration
    Liu, Bo
    Kita, Hidetoshi
    Yogo, Katsunori
    SEPARATION AND PURIFICATION TECHNOLOGY, 2020, 239
  • [5] Template-free synthesis of mesoporous polymers
    Sang, Xinxin
    Peng, Li
    Zhang, Jianling
    Han, Buxing
    Xue, Zhimin
    Liu, Chengcheng
    Yang, Guanying
    CHEMICAL COMMUNICATIONS, 2014, 50 (60) : 8128 - 8130
  • [6] Synthesis of mesoporous hydroxyapatite nanoparticles using a template-free sonochemistry-assisted microwave method
    Tong Liang
    Jiangchao Qian
    Yuan Yuan
    Changsheng Liu
    Journal of Materials Science, 2013, 48 : 5334 - 5341
  • [7] Synthesis of mesoporous hydroxyapatite nanoparticles using a template-free sonochemistry-assisted microwave method
    Liang, Tong
    Qian, Jiangchao
    Yuan, Yuan
    Liu, Changsheng
    JOURNAL OF MATERIALS SCIENCE, 2013, 48 (15) : 5334 - 5341
  • [8] Formation mechanism of microwave synthesized LTA zeolite membranes
    Li, Yanshuo
    Liu, Jie
    Yang, Weishen
    JOURNAL OF MEMBRANE SCIENCE, 2006, 281 (1-2) : 646 - 657
  • [9] Synthesis of template-free zeolite nanocrystals by reverse microemulsion-microwave method
    Chen, ZW
    Li, S
    Yan, YS
    CHEMISTRY OF MATERIALS, 2005, 17 (09) : 2262 - 2266
  • [10] Preparation of LTA zeolite membranes with few non-zeolite pores using microwave heating
    Li Yanshuo
    Liu Jie
    Chen Hongliang
    Yang Weishen
    Lin Liwu
    CHINESE JOURNAL OF CATALYSIS, 2006, 27 (07) : 544 - 546
12345