Voltammetric determination of Ioxynil and 2-methyl-3-nitroaniline using C-18 modified carbon paste electrodes

被引:0
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作者
Faller, C
Meyer, A
Henze, G
机构
[1] UNIV KAISERSLAUTERN,FACHBEREICH CHEM,D-54228 TRIER,GERMANY
[2] UNIV TRIER,ABT ANORGAN & ANALYT CHEM,D-54228 TRIER,GERMANY
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中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The stripping voltammetric behaviour of Ioxynil and 2-methyl-3-nitroaniline has been studied by means of a C-18 modified carbon paste electrode. The analytes are preconcentrated under open-circuit conditions (Ioxynil at pH 3.9; 2-methyl-3-nitroaniline at pH 10). For the determination of Ioxynil and 2-methyl-3-nitroaniline 0.01 mol/l HCl and 1 mol/l KOH, respectively, have been used as supporting electrolyte. Under optimized conditions detection limits up to 0.1 mu g/ml Ioxynil and 0.3 mu g/ml 2-methyl-3-nitroaniline have been obtained. The methods have been applied to the determination of Ioxynil and 2-methyl-3-nitroaniline in drinking water.
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页码:279 / 283
页数:5
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