The Synthesis of Novel S-, S,S-, S,S,S-, S,O-, N,S-Substituted Halogenobuta-1,3-dienes

被引：0

作者：

Ibis, Cemil ^{[1
]}

Ozkok, Funda ^{[1
]}

机构：

[1] Istanbul Univ, Fac Engn, Dept Chem, TR-34320 Avcilar, Turkey

来源：

ACTA CHIMICA SLOVENICA | 2012年 / 59卷 / 02期

关键词：

1,3-Butadiene; thioethers; N; S-substituted nitrodienes; crystal structure; NITROBUTADIENES; DERIVATIVES; DIENES; 2-NITRODIENES; CHEMISTRY;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

In this work, thiosubstituted nitrodiene compounds (3, 4a, 5a, b, 6c, 7a, 7c, 9) we re obtained from the reactions of some thiols with 2-nitropentachloro-1,3-butadiene. N,S-Substituted nitrodiene compounds (11a-g, 13, 15) we re obtained from 2-nitropentachloro-1,3-butadiene and some amines (morpholine and piperazine derivatives). The compound 4a was crystallized in the triclinic crystal system (space group P-1) with the unit cell parameters a = 6.6525(7) angstrom, b = 10.7906(5) angstrom, c = 10.8339(4) angstrom, alpha = 72.57(3)degrees, beta = 84.23(4)degrees, gamma = 75.81(3)degrees, V = 719.03(9) angstrom(3), Z = 2. The no vel compounds were characterized by elemental analysis, UV-VIS, FT-IR, H-1-NMR, NMR (C-13 or APT) and mass spectros copy.

引用

页码：294 / 301

页数：8

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