Some new organotin(IV) complexes:: synthesis and characterization by means of IR, 1H-, 13C-NMR and FAB-mass spectral studies

被引：0
|
作者：
Dubey, Raj Kumar [1 ]
Pathak, Sumit [1 ]
机构：
[1] Univ Allahabad, Dept Chem, Synthet Inorgan Metalloorgan Res Lab, Allahabad 211002, Uttar Pradesh, India
来源：
PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES INDIA SECTION A-PHYSICAL SCIENCES | 2008年 / 78A卷
关键词：
synthesis; tin (IV) complexes; IR; NMR; FAB-mass;
D O I：
暂无
中图分类号：
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号：
07 ; 0710 ; 09 ;
摘要：
Tri-n-butyltin(IV) complexes, containing Schiff bases, of the types [(sb) Bu-3(n) Sn(L)] [where sb = Schiff bases; salicylidene-4-methyl-1-aminobenzene (p-smabH), salicylidene-3-nitro-1-aminobenzene (snabH), 3-nitrobenzylidene-thiosemi-carbazide (nbts) and L=gamma -picoline (gamma-pic), pyridine (py), quinoline (qui), p-hydroxybenzaidehyde (p-hbaH), p-hydroxyacctophenone (p-haphcH), thiophenol (thiophH)] have been synthesized and characterized by elemental analyses and spectral (IR, H-1, C-13-NMR and FAB-mass) studies. These compounds are found to be coloured viscous liquids and are soluble in common organic solvents. On the basis of these studies the coordination site(s) are confirmed and their structures are also proposed tentatively.
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页码：197 / 202
页数：6
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