Crystal structure of 5,17-di-t-butyl-25,26,27,28-tetrahydroxy-11,23-(3-oxo-pentano)-calix[4]arene hydrate, C41H46O5 • 0.29H2O

被引:0
|
作者
Paulus, EF
Böhmer, V
O'Sullivan, P
机构
[1] Univ Frankfurt, Inst Mineral Kristallog, D-60325 Frankfurt, Germany
[2] Univ Mainz, Abt Lehramt Chem, Fachbereich Chem & Pharm, D-55099 Mainz, Germany
关键词
D O I
暂无
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
C41H46.58O5.29, monoclinic, P12(1)/n1 (No. 14), a = 13.350(3) Angstrom, b = 18.189(4) Angstrom, c = 14.842(3) Angstrom, beta = 94.54(3)degrees, V = 3592.7 Angstrom(3), Z = 4, R-gt(F) = 0.059, wR(ref)(F-2) = 0.156, T = 293 K.
引用
收藏
页码:141 / 143
页数:3
相关论文
共 50 条
  • [1] Crystal structure of 5,17-di-t-butyl-25,26,27,28-tetrahydroxy-11,23-(2-hydroxy-5-nitro-1, 3-xyleno)-calix[4]arene methylenechloride, C44H45NO7 • CH2Cl2
    Paulus, EF
    Böhmer, V
    O'Sullivan, P
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2002, 217 (01): : 144 - 146
  • [2] Crystal structure of 5,17-bis-cyano-25,26,27,28-tetrapropyloxy-calix[4]arene, C42H46N2O4
    Elaieb, Fethi
    Semeril, David
    Matt, Dominique
    Hedhli, Ahmed
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2016, 231 (03): : 943 - 945
  • [3] Synthesis and Crystal Structure of 5,17-Diformyl-11,23-di(tert-butyl)-25,26,27,28-tetrapropoxy-calix[4]arene
    Li Zheng-Yi
    Lai Yuan
    Shi Song
    Han Chen
    Chen Liang
    Sun Xiao-Qiang
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2013, 32 (09) : 1387 - 1391
  • [4] Synthesis and Crystal Structure of 5,17-Diformyl-11,23-di(tert-butyl)25,26,27,28-tetrapropoxy-calix[4]arene
    李正义
    来源
    石嵩
    韩辰
    陈亮
    孙小强
    结构化学, 2013, 32 (09) : 1387 - 1391
  • [5] Crystal structure of 5,17-dibromo-25,26,27,28-tetramethoxycalix[4]arene, C32H30Br2O4
    Hu, Xiao-Jun
    Zhang, Pin
    Li, Yong
    Yang, Hai-Jun
    Wang, Ru-Ji
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2007, 222 (04): : 405 - 406
  • [6] Crystal structure of 5,17-diformyl-25,26,27,28-tetrahydroxycalix[4]arene- dichloromethane, C31H26Cl2O6
    Wu, Chong
    Liu, Xiao-Long
    An, Rui
    Yang, Ye
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2020, 235 (06): : 1349 - 1350
  • [7] Crystal structure of 5,17-dinitro-25,26,27,28-tetrahydroxy-2,8,14,20-tetrathiacalix[4]arene - tetrahydrofuran (1:2), C24H14N2O8S4•2C4H8O
    Hu, Xiao-Jun
    Liu, Xiao
    Zhang, Pin
    Sun, Tie-Heng
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2008, 223 (04): : 393 - 394
  • [8] Crystal structure of 5,17-bis(N-tert-butylhydroxyamine)-11,23-dibromo-25,26,27,28-tetrapropoxycalix[4]arene, C48H64Br2N2O6
    Zhang, H.
    Hu, X. -J.
    Liu, J. -K.
    Li, Y.
    Yang, H. -J.
    Wang, R. -J.
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2006, 221 (02): : 203 - 205
  • [9] Crystal structure of 5-di-tert-butylphosphinoyl-25,26,27,28-tetrabenzoyloxy-calix[4]arene - dichloromethane (1:1), C64H65O5P - CH2Cl2, C65H67Cl2O5P
    Elaieb, Fethi
    Semeril, David
    Matt, Dominique
    Hedhli, Ahmed
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2015, 230 (02): : 174 - 176
  • [10] Crystal structure of 5,17-bis(N-tert-butylhydroxyamine)-25,26,27,28-tetrapropoxycalix[4]arene,C48H66N2O6
    Hu, X. -J.
    Yang, H. -J.
    Liu, J. -K.
    Zhang, H.
    Li, Y.
    Luo, Y. -H.
    Wang, R. -J.
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2006, 221 (03): : 329 - 331