Validation of a sampling procedure

被引：16

作者：

Bodnar, Malgorzata ^{[1
]}

Namiesnik, Jacek ^{[1
]}

Konieczka, Piotr ^{[1
]}

机构：

[1] Gdansk Univ Technol, Fac Chem, Dept Analyt Chem, PL-80233 Gdansk, Poland

来源：

TRAC-TRENDS IN ANALYTICAL CHEMISTRY | 2013年 / 51卷

关键词：

Analysis of variance; ANOVA; Experimental estimate; Measurement uncertainty; Modeling; Sampling; Sampling uncertainty; Uncertainty; Uncertainty budget; Validation; MEASUREMENT UNCERTAINTY;

D O I：

10.1016/j.trac.2013.06.011

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Each step of the analytical procedure influences the final results in a significant way. In the majority of cases, the analytical procedure encompasses sampling because the analysis of the entire object (material) is usually impossible, so it is necessary to include the uncertainty related to sampling procedure in the uncertainty-budget calculations. This article describes two basic ways of estimating sampling uncertainty (i.e. experimental and modeling). There is also an example that shows how to estimate uncertainty using analysis of variance (ANOVA). (C) 2013 Elsevier Ltd. All rights reserved.

引用

页码：117 / 126

页数：10

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