New Au(III), Pt(II) and Pd(II) complexes with glycyl-containing homopeptides

被引：18

作者：

Koleva, Bojidarka B. ^{[1
]}

Zareva, Sonya ^{[2
]}

Kolev, Tsonko ^{[3
]}

Spiteller, Michael ^{[3
]}

机构：

[1] Ruhr Univ Bochum, Lehrstuhl Analyt Chem, D-44780 Bochum, Germany

[2] Univ Sofia, Sofia 1164, Bulgaria

[3] Univ Dortmund, Inst Umweltforsch, D-44221 Dortmund, Germany

来源：

JOURNAL OF COORDINATION CHEMISTRY | 2008年 / 61卷 / 22期

关键词：

Glycyl-containing homopeptides; Au(III); Pd(II); Pt(II); Cisplatin; Complexes; Solid-state linear polarized IR-spectroscopy; UV-Vis; EPR; Quantum chemical calculations; H-1- and C-13 NMR; ESI MS; TGA and DSC; HPLC-MS-MS;

D O I：

10.1080/00958970802108817

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Twelve new Au(III), Pt(II) and Pd(II) complexes with glycyl-containing homopeptides glycyl-glycine (G2), glycyl-glycyl-glycine (G3), glycyl-glycyl-gycyl-glycine (G4), glycyl-glycyl-glycyl-glycyl-glycine (G5) and glycyl-glycyl-glycyl-glycyl-glycyl-glycine (G6) have been synthesized, isolated and characterized spectroscopically and structurally by means of solid-state linear-dichroic infrared (IR-LD) spectroscopy of oriented colloids in nematic liquid crystal host, H-1- and C-13-NMR, TGA and DSC, UV-Vis spectroscopy, EPR, ESI- and FAB mass spectrometry and HPLC tandem mass spectrometry (HPLC-MS/MS). Quantum chemical calculations are carried out with a view to obtain the structures and spectroscopic properties of the ligand and newly synthesized metal complexes.

引用

页码：3534 / 3548

页数：15

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