Rapid characterisation of flavonoids from Sophora alopecuroides L. by HPLC/DAD/ESI-MS n

被引：11
|
作者：
Yang, Wen-zhi [1 ]
Ye, Guan [2 ]
Meng, A-hui [3 ]
Sabir, Gulnar [4 ]
Qiao, Xue [1 ]
Guo, De-an [1 ]
Ye, Min [1 ]
机构：
[1] Peking Univ, Sch Pharmaceut Sci, State Key Lab Nat & Biomimet Drugs, Beijing 100191, Peoples R China
[2] NIH, Bethesda, MD 20892 USA
[3] Beijing Forestry Univ, Coll Biol Sci & Biotechnol, Beijing 100083, Peoples R China
[4] Xinjiang Inst Chinese Mat Med & Eth, Urumqi 830002, Peoples R China
来源：
NATURAL PRODUCT RESEARCH | 2013年 / 27卷 / 4-5期
关键词：
Sophora alopecuroides L; HPLC; DAD; ESI-MS; (n); characterisation; flavonoids; IONIZATION MASS-SPECTROMETRY; PHENOLIC-COMPOUNDS; AGLYCONES;
D O I：
10.1080/14786419.2012.688052
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
An HPLC/DAD/ESI-MS (n) method was established to characterise flavonoids in the seeds of Sophora alopecuroides L. All the flavonoids exhibited abundant [MH] ions, which triggered data-dependent multistage mass spectrometry fragmentations. Characteristic UV spectra were used to confirm flavonoid subtypes. In total, 22 flavonoids and two phenolic compounds were detected and identified. Five of them were identified by comparing with reference standards, and the others were characterised based on the retention behaviour, multistage fragmentation feature and UV absorption. A total of 19 compounds were reported from S. alopecuroides for the first time. This method accomplished rapid profiling of flavonoid constituents in S. alopecuroides L.
引用
收藏
页码：323 / 330
页数：8
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