Heterocycles with a β-nitroenamine fragment 1.: Synthesis of 2-amino-3-nitropyrans from nitroacetonitrile.: Crystal and molecular structure of 2-amino-4-(4-fluorophenyl)-3-nitro-7,7-dimethyl-5,6,7,8-tetrahydrochromen-5(4H)-one

被引:7
|
作者
Kislyi, VP
Nesterov, VN
Shestopalov, AM
Semenov, VV
机构
[1] ND Zelinskii Inst Organ Chem, Moscow 117913, Russia
[2] AN Nesmeyanov Organoelement Cpds Inst, Moscow 117813, Russia
关键词
arylidenenitroacetonitriles; 2-amino-3-nitropyrans; X-ray diffraction analysis;
D O I
10.1007/BF02496015
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Reactions of dimedone and dihydroresorcinol with arylidenenitroacetonitriles yield fused 2-amino-3-nitropyrans. The crystal and molecular structure of one of the reaction products was determined by X-ray diffraction analysis.
引用
收藏
页码:1131 / 1134
页数:4
相关论文
共 50 条
  • [1] Heterocycles with a β-nitroenamine fragment1. Synthesis of 2-amino-3-nitropyrans from nitroacetonitrile. Crystal and molecular structure of 2-amino-4-(4-fluorophenyl)-3-nitro-7,7-dimethyl-5,6,7,8-tetrahydrochromen-5(4H)-one
    V. P. Kislyi
    V. N. Nesterov
    A. M. Shestopalov
    V. V. Semenov
    Russian Chemical Bulletin, 1999, 48 : 1131 - 1134
  • [2] Ethyl 2-amino-4-(4-fluorophenyl)-7,7-dimethyl-5-oxo-5,6,7,8-tetrahydro-4H-benzo[b]pyran-3-carboxylate
    Shi, DQ
    Zhang, S
    Wang, XS
    Zhuang, QY
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 : O1501 - O1502
  • [3] 2-Amino-4-(2-methoxyphenyl)-7,7-dimethyl-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile and 2-amino-4-(2-methoxyphenyl)-7,7-dimethyl-3-nitro-4,6,7,8-tetrahydro-5H-chromen-5-one hemihydrate
    Nesterov, VN
    Kislyi, VP
    Sabutis, JL
    Nesterov, VV
    Wiedenfeld, DJ
    Semenov, VV
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2005, 61 : O741 - O744
  • [4] 2-Amino-4-(4-chlorophenyl)-7,7-dimethyl-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile
    Low, JN
    Cobo, J
    Nogueras, M
    Sánchez, A
    Quiroga, J
    Cisneros, C
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2003, 59 : O38 - O39
  • [5] 2-Amino-4-(4-chlorophenyl)-7,7dimethyl-5-oxo- 5,6,7,8-tetrahydro-4Hchromene-3-carbonitrilepropan-2-one monosolvate
    Mohamed, Shaaban K.
    Akkurt, Mehmet
    Tahir, Muhammad N.
    Abdelhamid, Antar A.
    Albayati, Mustafa R.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1965 - +
  • [6] Crystal structure of 2-amino-4-(4-fluorophenyl)-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile, C16H13FN2O2
    Meng, Xian-Fang
    Liu, Li-Zeng
    Bai, Zheng-Chen
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2016, 231 (02): : 455 - 456
  • [7] 2-Amino-4-(2-chlorophenyl)-7,7-dimethyl-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile hemihydrate
    Hu, Xiao-Lei
    Wang, Zhong-Xia
    Wang, Fang-Ming
    Han, Guang-Fan
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O823 - U2862
  • [8] 2-Amino-4-(4-methoxyphenyl)-7,7-dimethyl-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile propan-2-one monosolvate
    Mohamed, Shaaban K.
    Akkurt, Mehmet
    Tahir, Muhammad N.
    Abdelhamid, Antar A.
    Allahverdiyev, M. A.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O2206 - +
  • [9] 2-Amino-4-(1-naphthyl)-5-oxo5,6,7,8-tetrahydro-4H-chromene3-carbonitrile and 2-amino-7,7-dimethyl-4-(1-naphthyl)-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile
    Nesterov, VN
    Wiedenfeld, DJ
    Nesterova, SV
    Minton, MA
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2004, 60 : O334 - O337
  • [10] The synthesis and crystal structure of 2-amino-7,7-dimethyl-4-phenyl-5-oxo-5,6,7,8-tetrahydro,4-H-chromene-3-carbonitrile
    Gao, Y
    Cui, GY
    Guo, ZB
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2001, 20 (06) : 505 - 507