Microwave-assisted synthesis of copper oxide nanoparticles by apple peel extract and efficient catalytic reduction on methylene blue and crystal violet

被引:27
|
作者
Rajamohan, Rajaram [1 ]
Lee, Yong Rok [1 ]
机构
[1] Yeungnam Univ, Sch Chem Engn, Organ Mat Synth Lab, Gyeongson 38541, South Korea
关键词
Microwave -assisted synthesis; Apple peel; CuO NPs; XPS analysis; Organic dyes; Nanocatalytic reduction; MEDIATED GREEN SYNTHESIS; LEAF EXTRACT; GOLD NANOPARTICLES; SILVER NANOPARTICLES; CUO NANOPARTICLES; AQUEOUS EXTRACT; IN-SITU; REUSABLE CATALYST; RAPID SYNTHESIS; WASTE-WATER;
D O I
10.1016/j.molstruc.2022.134803
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Copper oxide nanoparticles (CuO NPs) can be synthesized by a one-pot synthetic process using microwave irradiation and an extract of apple peel as a nontoxic reducing agent and capping agent. This process has many advantages, including ease of operation, easy use of natural and non-toxic precursors, and the absence of harmful reagents. FE-SEM, FE-SEM, HR-TEM, XRD, XPS, Raman, and TGDTA are commonly used to characterize synthesized NPs. Based on the XRD results, the structure is face-centered cubic (FCC) with orientation (111). In addition, the synthesized green CuO NPs have been found to be highly effective in the reduction of MB dyes as well as CV dyes. Recovering and reusing catalysts with almost no loss of activity is possible.(c) 2022 Elsevier B.V. All rights reserved.
引用
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页数:10
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