Novel cyclic ultrasound-assisted liquid phase exfoliation of graphene in deionized water: A parameter study

被引:10
|
作者
Gao, Minhui [1 ,2 ]
Zong, Hu [1 ,2 ]
Li, Yifei [2 ]
Zhou, Ying [1 ]
Yu, Lei [2 ]
Qin, Ling [2 ,3 ]
Zhao, Su [2 ]
机构
[1] Zhejiang Univ Technol, Coll Chem Engn, Hangzhou 310014, Peoples R China
[2] Chinese Acad Sci, Ningbo Inst Ind Technol, Ningbo 315201, Peoples R China
[3] Univ Hull, Sch Engn, Cottingham Rd, Kingston Upon Hull HU6 7RX, England
关键词
Ultrasound-assisted liquid phase exfoliation; Graphene; Frequency; Circulation;
D O I
10.1016/j.matlet.2023.134011
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In this study, a novel cyclic ultrasound-assisted liquid phase exfoliation method for graphene in deionized water (DIW) was studied. A cyclic apparatus that can control temperature was developed. The size, thickness, number of layers of as-prepared graphene suspensions were characterized and quantified based on this apparatus covering the frequency range of 20 kHz to 35 kHz. The statistics shown that the prepared graphene has a surface area of 9.77 mu m2 and a composite conductivity of 1.45 x 104 S/m at a frequency of 35 kHz. This study offers a potential pathway for its large-scale production at a low cost.
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页数:4
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