A novel primitive cubic Al-Fe-Si phase in an Al-0.5Fe-0.2Si (wt.%) alloy

被引:2
|
作者
Dubaux, D. [1 ,3 ,4 ]
de Weerd, M. -C [1 ,3 ,4 ]
Ghanbaja, J. [1 ,3 ,4 ]
Bruyere, S. [1 ,3 ,4 ]
Redjaimia, A. [1 ,5 ]
Migot, S. [1 ,3 ,4 ]
Boulet, P. [1 ,3 ,4 ]
Sturm, S. [2 ,3 ,4 ,6 ,7 ]
Parapari, S. Semsari [2 ,3 ,4 ]
Fournee, V. [1 ,3 ,4 ]
Sicot, M. [1 ,3 ,4 ]
Ledieu, J. [1 ,3 ,4 ]
机构
[1] Univ Lorraine, CNRS, IJL, F-54000 Nancy, France
[2] Jozef Stefan Inst, Dept Nanostruct Mat, Jamova Cesta 39, Ljubljana 1000, Slovenia
[3] Univ Lorraine, Int Associated Lab PACS2, CNRS, Nancy, France
[4] Jozef Stefan Inst, Ljubljana, Slovenia
[5] Univ Lorraine, Lab Excellence Design Alloy Met Low Mass Struct DA, F-57070 Metz, France
[6] Jozef Stefan Int, Postgrad Sch, Jamova Cesta 39, Ljubljana 1000, Slovenia
[7] Univ Ljubljana, Fac Nat Sci & Engn, Dept Geol, Askerceva Cesta 12, Ljubljana 1000, Slovenia
来源
关键词
Characterization; Electron microscopy; Aluminum alloys; Intermetallics; Grain and interfaces; Phase transformation; AUTOMATED DIFFRACTION TOMOGRAPHY; INTERMETALLIC COMPOUND FORMATION; CRYSTAL-STRUCTURE; TERNARY-SYSTEM; MICRODIFFRACTION; SOLIDIFICATION;
D O I
10.1016/j.mtcomm.2023.107877
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
We report the identification of a new ternary Al-Fe-Si phase synthesized by arc-melting. Energy dispersive X-ray spectroscopy measurements show an homogeneous chemical distribution within the intermetallic grain with an overall stoichiometry equal to Al81.0Fe13.6Si5.4 (at.%). Atomically resolved High-Angle Annular Dark Field images collected along the [001] zone-axis are consistent with a cubic structure with an unit cell parameter close to 8.9 angstrom. Using microdiffraction analysis, it was possible to explore the zero-order Laue zone (ZOLZ) and first-order Laue zone (FOLZ) . This electron diffraction characterization leads to the conclusion that the Al81.0Fe13.6Si5.4 (at.%) crystallizes in the Pm (3) over bar space group.
引用
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页数:6
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