Copper Ferrite nanoparticles synthesised using a novel green synthesis route: Structural development and photocatalytic activity

被引:24
|
作者
Udhaya, P. Aji [1 ]
Ahmad, Awais [2 ]
Meena, M. [3 ]
Queen, M. Abila Jeba [1 ]
Aravind, M. [4 ]
Velusamy, P. [5 ]
Almutairi, Tahani Mazyad [6 ]
Mohammed, Abdallah. A. . A. . [6 ]
Ali, Shafaqat [7 ,8 ]
机构
[1] Holy Cross Coll, Dept Phys, Nagercoil, Tamil Nadu, India
[2] Univ Cordoba, Dept Quim Organ, Edificio Marie Curie C3,Ctra Nnal 4-A,Km 396, E-14014 Cordoba, Spain
[3] ST Hindu Coll, Dept Phys, Nagercoil, India
[4] Natl Engn Coll, Dept Phys, Kovilpatti, Tamil Nadu, India
[5] Thiagarajar Coll Engn, Dept Phys, Madurai 625015, Tamil Nadu, India
[6] King Saud Univ, Coll Sci, Dept Chem, Riyadh 11451, Saudi Arabia
[7] Govt Coll Univ, Dept Environm Sci, Faisalabad 38000, Pakistan
[8] China Med Univ, Dept Biol Sci & Technol, Taichung 40402, Taiwan
关键词
CuFe; 2; O; 4; nanoparticles; Ferrite; Green synthesis; Egg white; Rhodamine B; MAGNETIC-PROPERTIES; RHODAMINE-B; CUFE2O4; NANOPARTICLES; DEGRADATION; ZNFE2O4;
D O I
10.1016/j.molstruc.2022.134807
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
The copper ferrite nanoparticles, recognized for their ferromagnetic characteristics, minimal conductiv-ity, and superior electrochemical stability, were synthesized by a facile auto combustion approach using egg white as fuel via a green synthesis route. CuFe2O4 nanoparticles' structural, morphological, and op-tical properties were examined. XRD is used to determine the phase formation, particle size, and lattice parameter of spinel ferrite. X-ray Diffractometer (XRD), Fourier Transform Infrared Spectrometer (FTIR), Scanning Electron Microscopy (SEM), and Energy Dispersive X-ray analysis were used to rigorously ex-amine the phase purity of the synthesized spinel ferrite. For morphological analysis, SEM and TEM were employed, whereas EDAX was used for elemental analyses. For a better knowledge of the conduction band (CB) and valence band (VB) boundaries of the produced nanoparticles, optical experiments were conducted by UV Diffuse Reflectance Spectroscopy. The degradation of Rhodamine B dye determined the photocatalytic competence of the synthesized sample under visible light. At regular intervals of time, the entire process was observed with a spectrophotometer. CuFe2O4 nanoparticles reveal a maximum photocatalytic degradation efficiency of around 94%, which is higher than that of CuFe2O4 nanoparticles prepared via other chemical route.(c) 2022 Published by Elsevier B.V.
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页数:7
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