CRYSTAL STRUCTURE OF 3-NITRO-2, 6-BIS（4'-BENZO-15-CROWN-5）-AMINOPYRIDINE POTASSIUM PICRATE HYDRATE METHANOL, (C33H42N4o12K)C6H2N3o7·H2O ·CH3OH

被引：0
|
作者：
Zhang Li-Tao Luo Bao-Sheng Lu Tian-Bao Hu Hong-Wen Zhang Shao-Hui Department of Chemistry
机构：
来源：
结构化学 | 1991年 / 03期
关键词：
BIS; N4o; AMINOPYRIDINE POTASSIUM PICRATE HYDRATE METHANOL; BENZO-15-CROWN-5; CRYSTAL STRUCTURE OF 3-NITRO-2; H2O; K)C6H2N3o7; CH3OH; OH;
D O I：
10.14102/j.cnki.0254-5861.1991.03.001
中图分类号：
学科分类号：
摘要：
The title compound, (C33H42N4O12K)C6H2N3O7·H2O·CH3OH,Mr = 1003. 98,space group P1,a=11. 458(2) ,b= 14. 565(6) ,c=15. 828(3) A ;α=63. 34 (2),β=74. 06(1),γ=81. 03(2)°,V=2268. 1 A3;Z = 2,Dx = l. 47g/cm3,λ=0. 71069 A (MoKa).The final R = 0. 041 for 1700 observed reflections (I≥3σ(I)). The molecule is sandwich-like, and the cation K+ is sandwiched between the two crown rings.
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页码：167 / 170
页数：4
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