CRYSTAL STRUCTURE OF 2-ETHYLTHIO-β-NAPHOTHIAZOLE,C13H11S2N

被引：0
|
作者：
Wu Dingming Huang Chaosheng Wang Hongjun Lu Getan Wang Hongrui Fujian Institute of Research on the Structure of Matter
机构：
来源：
结构化学 | 1988年 / 03期
关键词：
CRYSTAL STRUCTURE OF 2-ETHYLTHIO; NAPHOTHIAZOLE; C13H11S2N;
D O I：
10.14102/j.cnki.0254-5861.1988.03.010
中图分类号：
学科分类号：
摘要：
The crystal structure of the title compound,intermediate of an organic dye,was determined by X-ray analysis for synthesis of the dye. C13H11S2N, Mr = 245.36, orthorhombic, P212121,a=8.827(3), b = 10.403(12),c=12.837(2) A, V = 1178.7(19) A3,Z=4, Dx=1.938 g.cm-3,λ(MoKα)= 0.71039 A, F(OOO) = 512, room temperature, R = 0.041. The results reveal that the naphthyl ring and thiazote ring in the compound are co-planar. The S(1) atom in -SC2H5 fork chain takes part in the big conjugation.
引用
收藏
页码：218 / 221
页数：4
相关论文
共 50 条
  • [1] Crystal structure N-tosyl-2-methylserine-β-lactone, C11H13NO4S
    Lauf, Carolin
    Bruhn, Clemens
    Frauenrath, Herbert
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2010, 225 (01): : 137 - 138
  • [2] CRYSTAL AND MOLECULAR STRUCTURE OF P2S2N5C2H13
    ZIEGLER, ML
    WEISS, J
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1968, 361 (3-4): : 136 - &
  • [3] CRYSTAL-STRUCTURE OF C13H13N2J
    LEVINA, OI
    KURKUTOVA, EN
    ILIUKHIN, VV
    BELOV, NV
    DOKLADY AKADEMII NAUK SSSR, 1976, 229 (03): : 604 - 606
  • [4] Crystal structure of N,N-diphenylformamide, C13H11NO
    Hosten, Eric C.
    Betz, Richard
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2021, 236 (01): : 57 - 59
  • [5] Crystal structure of L-tryptophanium phosphite, (C11H13N2O2)[H2PO3]
    Silva, MR
    Paixao, JA
    Beja, AM
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2005, 220 (03): : 487 - 488
  • [6] Crystal structure of N,N′-diphenylguanidinium acetate, C13H14N3+C2H3O2-
    Beja, AM
    Paixao, JA
    Silva, MR
    da Veiga, LA
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2000, 215 (04): : 579 - 580
  • [7] Crystal structure of N-benzylsalicylamide,C14H13NO2
    Liu, Sheng-Li
    Liang, En-Xiang
    Yu, Liang-Cai
    Huang, Li
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2007, 222 (04): : 433 - 434
  • [8] Crystal structure of N-tosyl-2-methylserine, C11H15NO5S
    Lauf, Carolin
    Bruhn, Clemens
    Frauenrath, Herbert
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2010, 225 (01): : 139 - 140
  • [9] Crystal structure of 4-phenylpiperazing-1-ium (4-phenylpiperazin-1-yl)carbothioylsulfanide, [C10H15N2][C11H13N2S2]
    Lo, Kong Mun
    Lee, See Mun
    Tiekink, Edward R. T.
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2019, 234 (06): : 1329 - 1331
  • [10] Crystal structure of dichloroacridinedimethylaminepalladium(II), PdCl2(C13H9N)(C2H7N)
    Ha, Kwang
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2010, 225 (04): : 655 - 656
12345